GCMS analysis results for sample AE08835, April 25, 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2202\8835.D Vial: 27 Acq On : 23 Apr 2002 10:58 am Operator: Sample : gc/ms scan 4/12 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.81 0.26 ug/1 44039 Naphthalene-d8 15.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 78 2 N-(Trif .oroacetyl)-0,0',0'•-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 3 3,4-Dih droxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 37 4 Noradrenaline, tetra-TMS_______ 457 C20H43NO3Si4 000000-00-0 32 Abundance Scan 1063 (14.806 min): 8835.D (-) m/z 73.00 100.00% 73

5000 267 355

14.40 14.60 14.80 15.00 15.20 45 , , 133154 191 223 „ 323 1 ■ ■' i ‘ ■ ——————— m/z 355.05 45.25% miz-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 267.00 45.03% ■ * । * > * * । * ... 207 . .323 mz->____ 50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacetyl)-O,0 ‘,0"-tris(trimethylsily!)no 73 T — 355 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.05 13.29%

45 ■ ■ i |, 126147 193.. 265 .1376. 481 miz-> 50 100 150 200 250 300 350 400 450 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- T T 73 14.40 14.60 14.80 15.00 15.20 m/z 268.00 10.79%

5000 267 179 356 45 147 209 237 , 312 ■ ‘i ‘ ■ JU 11t i ■ ' ■ ' i ■ ‘ ■ i • ■ i ■ ' ' ' i ■ ■ m/z—> 50 100 150 200 250 300 350 400 450 14.40 14.60 14.80 15.00 15.20

8835.D GCMS0412.M Tue Apr 23 14:25:05 2002 Page 2

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