GCMS analysis results for sample AE06413, April 23, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\APR04 05\6413.D Vial: 8 Acq On 5 Apr 2002 6:54 pm Operator: Sample gc/ms scan 3/19 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************************* * * Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 14.84 0.55 ug/1 84419 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H30O5Si5 000541-02-6(87 2 N- (Trifluoroacetyl) -0,0' ,O' '-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 3 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38 4 Phenethylamine, N-methyl-.beta. ,3,4 399 C18H37NO3Si3 010538-85-9 38 Abundance < Scan 1067 (14.844 min): 6413.D (-) m/ z 73.00 100.00% 73

5000 267 355

• • i * ■ • i ■ ■ 45I 1 14.60 14.80 15.00 15.20 103 133 162 191p* —I’ 223 , i ■ ■ । 323 । “( ■ ■ ■ । ■ ■ ■ ■ । • m/z 267.00 45.35% iz-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 / 5000 3I 1 4 ′ 1d.8 14.60 14.80 15,00 15.20 m/z 355.05 45.27% 4 • 1 323, 1 mz-> 50 100 ' ‘ 150' 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacety!)-O,0’,0"-tris(trimethylsilyl)no 73 - 355 14.60 14.80 15.00 15.20 5000 m/z 356.05 14.93%

45 ■ I 1 126147, 193....... 265 'i ’ ■ 1 376 481 mlz-> 50 ' 100 ' 150 200 250 300 350 400 '450 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 14.60 14.80 15.00 15.20 m/z 357.05 10.38% 5000 267 179 356 45 147

z—> _L 1 ’ 1 1 ’ ‘ 50 1, 209 237 , , , , 312 ,M.......... I****I*II[ 100 150 200 250 300 350 400 450 * • i * ’ I* 14.60 14.80 15.00 15.20

6413.D GCMS0408.M Wed Apr 10 12:22:53 2002 Page 1

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