GCMS analysis results for sample AE06429, April 23, 2002

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Data File C:\HPCHEM\1\DATA\APR04 05\6429.D Vial: 15 Acq On 6 Apr 2002 3:47 am Operator: Sample gc/ms scan 3/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.85 0.81 ug/1 119508 Naphthalene-d8 15.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 52 2 Phenethy/amine, N-methyl-.beta., 3,4 399 C18H37NO3Si3 010538-85-9 38 3 N- (Trifluoroacety1) -0,0' ,0’ '-tris (t 481 C19H34F3NO4S13 000000-00-0 38 4 N-(Trif/uoroacetyl)-N,0,0',0'1-tetr 553 C22H42F3NO4Si4 000000-00-0 38 Abundance Scan 1068 (14.848 min): 6429.D (-) m/z 73.00 100.00% 73

267 355 5000

1 rI 1 1 ■ ■ i ■ ■ ■ • i ■ ■ 45 14.60 14.80 15.00 15.20 - _ 133154 193, 2371 .......... m/z 355.05 57.41% mlz-> 50 100 150 200 250 300 ' 350 ' ‘460 ' 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.60 14.80 15.00 15.20 m/z 266.95 54.07% —1k ................ 207 323 I "nfz-> 50 100 150 200 250 300 350 400 450 Abundance #53791: Phenethylamine, N-methy!-.beta.I3,4-tris(trimethyls 3$5 ■ ■ i ■ ■ 1 1 i ■ • ■ ‘ i • • 14.60 14.80 15.00 15.20 5000 73 m/z 356.05 19.56%

51 1 147 179 267 294 384 ■ i' ■ ■ • ■ i ■

mlz-> 50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacetyl)-O,O’,0"-tris(trimethylsilyl)no TT-p-r-r-r-p-r ■ • i 1 1 ‘ 1 i * 73 14.60 14.80 15.00 15.20 355 m/z 267.90 14.53% 5000

45 'i 1 1 I 126147 193 ...... 265 376.481 miz—> 50 . 100 ' ' 150 200 250 300 350 400 450 ' 14.60 14.80 15'00 15.20

6429.D GCMS0408.M Wed Apr 10 12:24:18 2002 Page 2

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