GCMS surrogate recovery data for sample AE06426, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\APR04 05\6426.D Vial: 12 Acq On 5 Apr 2002 11:51 pm Operator: Sample gc/ms scan 3/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 14.85 0.26 ug/1 39984 Naphthalene-d8 15.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual ----------------------- ) 1 Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 90 2 N- (Trifluoroacetyl) -N, 0,0' ,0' '-tetr 553 C22H42F3NO4Si4 000000-00-0 38 3 Phenethylamine, N-methyl-.beta. , 3,4 399 C18H37NO3Si3 010538-85-9 32 4 N-(Trifluo/acetyl) -0,0’,0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 32 Abundance Scan 1068 (14.848 min): 6426. D (-) m/z 73.00 100.00% 73

267 355 5000

TTEI ■ 1 i • ■ 1 ■ । > ।

45 14.60 14.80 15.00 15.20 ' 'I t ‘ i ■ ■ ■ ' i ' 1 ' 193i ' 1 1 i 1 ' ' ' i ■ ■ • ■ i I ' • ■ ' i • ' ' • i ' ' ■ ' i ' ' ‘ ' i ■ 1 m/z 355.05 - 54.27% mlz—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 1 1 । 1 111। > ''> । । । 1 । । । । 14.60 14.80 15.00 15.20 m/z 2 67.00 51.50% .......................... 207 323, m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethyIsi 73

355 14.60 14.80 15.00 15.20 5000 m/z 356.05 17.31%

45 L_ T I I I • I 147 193 267 538 1 1 i 1 TI I I I T[ I I I I I TT 1 I [ I I I ! TT I I I [ I—T ' 1 ' i 1 ' ' ‘ I ' 1 ' 1 i ' 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 14.60 14.80 15.00 15.20 m/z 357.05 12.50%|

5000 355 44 i, . । . 147 193 267 294 - 111 TLII 1 1 1 TBT I I I Tnm I 13 I ′ TT I TIm TTn[m I I T I I—I TI——T—TI—1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

6426.D GCMS0408.M Wed Apr 10 12:23:45 2002 Page 1

NYC-WTC_000039701