GCMS analysis results for sample AE08018, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1102\8018.D Vial: 24 Acq On : 12 Apr 2002 1:00 pm Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.83 0.36 ug/1 39620 Naphthalene-d8 15.86

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 N-(Trifluora&etyl) -0,0',0"-tris(tri 495 C20H36F3NO4S13 000000-00-0 43 3 N- (Trifluoroacetyl) -N,0,0' ,0' '-tetr 553 C22H42F3NO4Si4 000000-00-0 43 4 Phenethylamin N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 37 Abundance m/ z 73.00 100.00% Scan 1066 (14.831 min): 8018.D (-) 73

355 5000 267

bBl 45 154 193 14.60 14.80 15.00 15.20 1 , m/z 355.05 53.65% ‘ 1 i ’ 1 1/1 1 i ' ' ' ' i ' 1 ' ' i ' ' ' ' i ' ■ ■ ■ i ' ■ ■ ■ i ' ' m/z->______ 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ■ ■ i ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ 14.60 14.80 15.00 15.20 m/ z 267.00 42.77% ......... 207 1 323, ———k n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(Trifluoracetyl)-O,O',O"-tris(trimethylsilyl)epin 73 355 1 1 ' 1 ■ 1 14.60 14.80 15.00 15.20 5000 m/z 356.05 18.08%

45 I 140 184 281 480 ‘ 'i 1 ' 1 1 i 1 ' i ' 1 1 ' i ■ ' 1 1 i ■ 1 ' 1 i ' 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi ■ ■ i > > ■ - । . I । । । 1 I > 1 73 14.60 14.80 15.00 15.20 m/z 267.90 12.74% 355 5000

45 l h 147 193 267 538 ■ 'i 1 ' III/‘/I//nI**IIIIIII"II ' I 1 1 1 ' I 1 1 ' ' I ' 1 ' ' I ' '1 1 1 1 1 1r-f-r 1 1 i ' ■ ■ ' i 1 1 ' 1 i 1 1 1 1 I ' 1 ' m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

8018.D GCMS0412.M Tue Apr 16 12:08:35 2002 Page 1

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