Laboratory report documenting GCMS analysis of sample AE08013 conducted on April 24, 2002, including surrogate recovery data.
NYC-WTC_000047673–000047681Folder label: “GCMS X 4/4/02 A 4/12/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\APR1102\8013.D Vial: 19 Acq On : 12 Apr 2002 8:04 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
14.83 0.55 ug/1 73523 Naphthalene-d8 15.87
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 N- (Trifluoroacety1) -N,O,O' ,0' '-tetr 553 C22H42F3NO4Si4 000000-00-0 47 3 N- (Trifluoracetyl) -0,0',0"-tris(tri 495 C20H36F3N04Si3 000000-00-0 38 4 Phenethylamine, N-methyl-.beta . , 3,4 399 C18H37NO3Si3 010538-85-9 38 Abundance Scan 1066 (14.829 min): 8013.D (-) m/z 73.00 100.00% 73
5000 267 355
45 14.40 14.60 14.80 15.00 15.20 108 154 193 223 , 323, m/z-> —4504 100 150 +-----1.4 ■ 200 250 300 350 400 450 500 550 m/z 267.00 40.23% Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 5000 267 । . . . . ! . , , ,/......... —....... , , , . , t . . . . । , 14.40 14.60 14.80 15.00 15.20 m/z 355.05 39.21% 207 | 3231 1" 1* ■ - i ■ ■ ■ ■ i ■ ■ ■ t ■ ■ ।
m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O,,O"-tetrakis(trimethylsi 73 ................../..................... 355 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.05 13.85%
45 | 147 193 267 538 1 'i 1 ′ 1 i ' 1 1 ' i ' ' ' ‘ i 1 ' ' ■ i ' ' ' ' i ' ■ ‘ ' i ■ 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(Trifluoracetyl)-O,O',O''-tris(trimethylsilyl)epin ' ' i ■ ' ■ r i ' 1 73 14.40 14.60 14.80 15.00 15.20 355 m/z 357.05 11.90% 5000
45 140 184 281 480 ■ ■ i ■ ' 1 1 ——— i ' i ■ 1 ' 1 i ' 1 T-r-[-r-r-r-i-|-r-r m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20
8013.D GCMS0412.M Tue Apr 16 12:07:14 2002 Page 1
NYC-WTC_000047680
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NYC-WTC_000047664
Laboratory report documenting GCMS analysis of sample AE08012 conducted on April 24, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047725
Laboratory report documenting GCMS analysis of sample AE08018 conducted on April 24, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047682
Laboratory report documenting GCMS analysis of sample AE08014 conducted on April 24, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046655
Laboratory report documenting GCMS analysis of sample AE07316 conducted on April 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049102
Gas chromatography-mass spectrometry analysis results for sample AE08760 including detection of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047061
DEP laboratory report showing GCMS analysis results for sample AE07504 conducted on April 23, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047008
DEP laboratory report showing GCMS analysis results for sample AE07498 conducted on April 23, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039703
Surrogate recovery data for sample AE06428 analyzed by GCMS on April 18, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039694
Surrogate recovery data for sample AE06426 analyzed by GCMS on April 18, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000040137
Laboratory report documenting GCMS analysis of sample AE06992 conducted on April 16, 2002, including surrogate recovery data.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000040079
Laboratory report documenting GCMS analysis of environmental sample AE06998 conducted on April 16, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000040128
Laboratory report documenting GCMS analysis of sample AE06993 conducted on April 16, 2002, including surrogate recovery data.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000047639
Department of Environmental Protection GCMS analysis record dated April 4-12, 2002.
Filed in the same folder
NYC-WTC_000047640
Fragmented page from a GCMS record dated April 12, 2002, containing method parameters and sample identifiers.
Filed in the same folder
NYC-WTC_000047643
Laboratory report of a GCMS blank analysis for sample AE08012 conducted on April 17, 2002, showing non-detect levels for various compounds.
Filed in the same folder
NYC-WTC_000047652
Laboratory report of GCMS calibration data for sample AE08012 conducted on April 17, 2002, listing target compounds and concentrations.
Filed in the same folder
NYC-WTC_000047656
Laboratory report of GCMS reference analysis for sample AE08012 conducted on April 17, 2002, showing recovery percentages for target compounds.
Filed in the same folder