GCMS analysis results for sample AE07315, April 2002

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Laboratory report documenting GCMS analysis of sample AE07315 conducted on April 10, 2002.

NYC-WTC_000046645–000046654

Folder label: “GCMS X 3/28/02 A 2/27/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\APR0 3 02\7315.D Vial: 11 Acq On 3 Apr 2002 10:34 pm Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 14.85 1.42 ug/1 199919 Naphthalene-d8 15.88 Hit# of 5 Tentative ID MW MolForm CAS# Dual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 37 3 N-(Trifluoroacetyl) -N,O,O',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 37 4 N-(Trifluoracetyl)-0,01,0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37 Abundance Scan 1068 (14.847 min): 7315.D (-) m/ z 73.00 100.00% 73 n

5000 267 355

1 1 I T" ' ■ - i ■ ■ ■ ■ । ■

45 14.60 14.80 15.00 15.20 125 154 193 223 , 323 ' । । l 1 i r i । ‘ ।’ । । । । । । ।"। । < '। T । 11gi I I 1 I 1 I I 1 [ I I I I I I I I I [' I I I I I I I m/z 355.05 48.48% m/z->____ 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000- 267 . /J . 14.60 14.80 15.00 15.20 m/ z 2 67.00 48.01%

—— ... . 207 .1 323, m/z->______ 50 100 150200 250 300 350 400 450 500 550 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 / \ 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 17.80% 44 147 193 267294 1 I 1 '' ' '■ i ■ 1 1 1 -i ’ 1 1 1 i 1 ■ ■ ■ i ■ '■ ■ '‘i 1 ' 1 ' i ' 1 1 1 i 1 1 I 1 ' Impni 1 1 I ' m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi ................ 73 14.60 14.80 15.00 15.20 m/z 2 68.00 12.67% 355 5000

m/z--> l 1 1 । 1T 50 100 । | ] | | । 147 i

150 | I-T । 193 r

200 | i i i i

250 | 267 i "i ( i

300 | I I i— i

350 | I I 1 IP71

400 I “I ']

450 I I " 1 "T |

500 1—T 538 550 4 14.60 14.80 15.00 15.20

7315.D GCMS0403.M Tue Apr 09 13:08:34 2002 Page 2

NYC-WTC_000046653

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GCMS analysis results for sample AE07318, April 2002 · Box DEP Box 27

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Laboratory report documenting GCMS analysis of sample AE07318 conducted on April 10, 2002.

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