GCMS analysis results for sample AE07314, April 2002

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Laboratory report documenting GCMS analysis of sample AE07314 conducted on April 10, 2002.

NYC-WTC_000046635–000046644

Folder label: “GCMS X 3/28/02 A 2/27/02”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\l\DATA\APR0302\7314.D Vial: 10 Acq On : 3 Apr 2002 9:34 pm Operator: Sample : gc/ms scan 3/28 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 14.84 1.09 ug/1 161463 Naphthalene-d8 15.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 N-(Trif luorcyacetyl)-N, 0,0 1,0 1 '-tetr 553 C22H42F3NO4Si4 000000-00-0 47 3 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 4 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 05 5429-85-1 38 Abundance 1 Scan 1067 (14.843 min): 7314.D (-) m/ z 73.00 100.00% 73

5000- 267 355 \ ........ ‘‘1 I 1 ’I I I I I 1 1 i ■ ■ 45 125 154 193 237 14.60 14.80 15.00 15.20 i । 323 1 '1 1 1 — ———————— m/z 355.05 44.20% m/z—>____ 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 / 5000- 14.60 14.80 15.00 15.20 m/z 267.00 44.11% ......... 207 1.., ,323, .... TII m/z-> 50 100 150 200 250 300 550 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi 73 ................. \...................... ■ ■ । ■ ■ ■ ■ । । 1 > । I ■ । ' । । । ' 355 14.60 14.80 15.00 15.20 5000 m/z 356.05 15.43%

45 I 1 ' i ' 1 r 147 193 267 ■ 'i 1 1 ■ ■' i 1 1 1 ■ i 1f 1 r1 1 1 1 । 538 1 ' ' i ' ' ■ ‘ i ' ' ' 1 i r r ■ ' i ' 1 m/z->____ 50 100 150 200 250 500 350 400 450 500 550 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls ----- 73 14.60 14.80 15.00 15.20 m/z 268.00 11.03% 5000 355 44 147 193 267 294 / ........ ———————————— ogtnuugvut i j i i ' i" i ' ] r I m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

7314.D GCMS0403.M Tue Apr 09 13:08:21 2002 Page 2

NYC-WTC_000046643

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GCMS analysis results for sample AE07315, April 2002 · Box DEP Box 27

NYC-WTC_000046645

Laboratory report documenting GCMS analysis of sample AE07315 conducted on April 10, 2002.

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