GCMS analysis results for sample AE07314, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0302\7314.D Vial: 10 Acq On 3 Apr 2002 9:34 pm Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 1 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.28 0.40 ug/1 46425 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130• 000918-00-3 38 2 Tetradecane, 1-chloro- 232 C14H29C1 002425-54-9 9 3 Hexyl octyl ether 214 C14H30O 000000-00-0 9 4 1 -Hexacosanol 382 C26H540 000506-52-5 9 Abundance Scan 352 (8,280 min): 7314.D (-) m/z 43.00 100.00% 43

5000

■ . . , . | , r | , , , I | 7 , , | I' I T—T

. 83 97 125 8.00 8.20 8.40 8.60 .......... ’I’’ i ’’, 61,1, I. „ II............ i ' 1 ■ ' i 1 ‘ 1 1 i 1 1 ■ ■ i 1 ■ ■ ■ i ■ ■ 1 ■ i 1 1 ■ ' i 1 CFTTRmETELTT m/z 124.85 11.81% m/z-> 20 40I 60 80 100 120 140 160 180 200 220 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 8.00 8.20 8.40 8.60 m/z 82.85 9.90% 15 85 97 125 1 '' i 1 r ■ 1 i T TT 1 i '' 1 1 '"i ' 1 1 1 i 1 1 1 1 i 1 ' 1 ' i ‘ ‘ i 1 ' 1 1 1 1 ' ' 1 i 1 ' 1 1 I m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #30366: Tetradecane, 1-chloro- 43 57

8.00 8.20 8.40 8.60 5000 m/z 96.95 9.63% 71 27 83 97 ... ■ i ■ ■ ■ ■ । ■ ■ ■ । । ■ ■ ■ ■ । ■ | I, 111................................... 196..........232 m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #26415: Hexyl octyl ether 43 57 85 8.00 8.20 8.40 8.60 m/z 127.00 9.06% 71

5000

112 — 1 ' I ' ' ‘ ' 1 1 1 1 1 r1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 8.00 8.20 8.40 8.60

7314.D GCMS0403.M Tue Apr 09 13:08:21 2002 Page 1

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