GCMS analysis results for sample AE09095, April 2002

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Laboratory report documenting GCMS analysis of sample AE09095 conducted on April 26, 2002.

NYC-WTC_000046480–000046496

Folder label: “GCMS X 4/17/02 A 4/24/02”

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NYC 9/11 Public Portal Document

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Data File C:\HPCHEM\l\DATA\APR03022\5845 .D Vial: 19 Acq On 4 Apr 2002 1:25 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

8.27 1.31 ug/1 63069 1,4-Dichlorobenzene-d4 12.25 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130> 000918-00-3 42 2 2-Acetyl-1,4,5,6-tetrahydropyridine 125 C7H11NO 000000-00-0 4 3 2-Propanone, 1,1-dichloro- 126 C3H4C1201 000513-88-2 4 4 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 3 Abundance Scan 352 (8.274 min): 5845. D (-) m/z 43.05 100.00% 43

5000

i ”I i i । i JA r > i । i i TrT i rr

' 1 i 1 1 1 1 i ' 35 -+ 49,55/63 ..... 83... %7...... 119177 1 1 '1 1 1 1 ' I ‘ ’ 1 1 I ■ ' 1 ' I r’ 1 • I ' ' 1 1 I 1 1 ' 1 p ' ■ ' I I ' ' ' I ' m/z 124.95 8.00 8.20 8.40 8.60 11.91% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 r i । । । r i । । । r r r । I I’IIII

8.00 8.20 8.40 8.60 m/z 96.85 8.19% 15 1U 35 49 ■ i ■ i t I I I I U IIa > I I I < 1 I I 85 j I I I I I I I 97 I I I I I I I I I 117 125 I I I I I ( I I I I I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4332: 2-Acetyl-1,4,5,6-tetrahydropyridine 43 54 82 8.00 8.20 8.40 8.60 5000 125 m/z 126.90 8.10%

1 — I I I I | I I TT ] I I I — I" T I I | T —in 1 1 ' . ..I . %7 , .110. | t———r m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4368: 2-Propanone, 1,1-dichloro- ' 1 ' ' i ' 1 ■ ' i ' 1 1 1 i ■ ■ ' r i ■ ■ ‘ r 43 8.00 8.20 8.40 8.60 m/z 82.95 7.77% 5000

15 I 27 37 1 49 .1. T[ I i i i 631........ _ 76 83 93 J , | i I i i [ ! I I r | i ■ i i | ■ I ■ i | I I I I | I I ’’I’ TT | I I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 8.00 8.20 8.40 8.60

5845.D GCMS0408.M Tue Apr 16 08:16:19 2002 Page 2

NYC-WTC_000046495

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NYC-WTC_000046495Source: NYC Law Department, mirrored locally

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