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GCMS calibration results for sample AE09585, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS calibration data for sample AE09585 generated on May 4-6, 2002.

NYC-WTC_000046294–000046302

Folder label: “GCMS X 5/7/02 A 5/9/02

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Scanned page image, NYC-WTC_000046300
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0302\9585.D Vial: 12 Acq On 4 May 2002 12:49 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 8.23 2.40 ug/1 153848 1,4-Dichlorobenzene-d4 12.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 43 2 2-Acetylthiazole 127 C5H5NOS 024295-03-2 12 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 4 Ethanol,/2,2,2 -trichlorq-________ 148 C2H3C130 000115-20-8 4 Abundance 7 Scan 348 (8.229 min): 9585.D (-) m/z 43.05 100.0o* 43

5000

।_ i i i i j t i 1 । i । i । [ i । । । 1 i r

61 82 97 , 125 7.80 8.00 8.20 8.40 8.60 36 - m/z 97.00 11.46% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 i 1 1 1 1 i 1 ■ 1 1 i 1 1 1 1 i 1 ' 1 1 i 1 1 ■ 7.80 8.00 8.20 8.40 8.60 m/z 124.95 10.69% 15 — 35 i | T 1 1 49 85 97 117 125 7 | i i i r | ‘II 1 ‘ | 1 ' 1 1 । i > i i । i i i i । I I > i । i t i"*i i i । । । r i I ■ 111 I 11111 | i I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #64976: 2-Acetylthiazole 43 — 7.80 8.00 8.20 8.40 8.60 5000 m/z 126.95 9.94% 127 58 99 112 85

m/z-> 34 ' i ■ 1 ’ ' i ■ 1 ■ ■ i ' 1 1 1 i ■ ■ ■ 1 i 1 I 11 11 i ‘ L ' 1 I 1 1 1 ri ■ ■ 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4732: N-Acetylpyrrolidone Tdn 1 i ' 1 1 1 i ' 1 I , —I 1 1 I I 1“ I ■ I ' I 43 7.80 8.00 8.20 8.40 8.60 m/ z 46.95 9.92% 5000

m/z--> 1 I 1 ' 1 ' I ' 1 ' 10 20 30 [ ■ ■ ' 1 I ' 30 40 1 H 50 56

60 69 II 70 86 99

112.......... I ' 110 '80i ' Il 90। ' , ' 100 120 130 127 1 _DMMMMA [ I ' I I I > I I I 7.80 8.00 8.20 I I I II I r I f I I 8.40 8.60 r —T

9585.D GCMS0501.M Mon May 06 10:50:44 2002 Page 2

NYC-WTC_000046300

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NYC-WTC_000046300Source: NYC Law Department, mirrored locally

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