Laboratory report documenting GCMS analysis of sample AE09451 including surrogate recovery data conducted on May 15, 2002.
NYC-WTC_000045516–000045525Folder label: “GCMS X 5/3/02 A 5/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\MAY0802\9451.D Vial: 11 Acq On 8 May 2002 8:21 pm Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
8.23 2.38 ug/1 162575 1,4-Dichlorobenzene-d4 12.20
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 28 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 3 Ethanol, 2,2,2-trichloro- 148 C2H3C130 000115-20-8 9 4 2 -Acetylthiazole 127 C5H5NOS 024295-03-2 5 Abundance L Scan 348 (8.227 min): 9451 D (-) m/ z 43.05 100.00% 43
5000
97 151-- 111'11II 1■1 r'।r'119177 , 63 82 7.80 8.00 8.20 8.40 8.60 ........................36 11111111''111' *1' । " m/z 126.95 12.40% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43
5000 7.80 8.00 8.20 8.40 8.60 m/z 97.00 12.01% 15 35 85 97 117 125 ■ ■ i ■ ■ ■ ■ i ■ ■' ' । 1 ■’> * I' 1 ''''i 1 1 'r i''' 1 i' 1 1 ‘ i' /z—> 10 20 30 40 50 60 70 80 ' r 1' ■ i1 ■111'11 ■ i'1 ■' j *' " । ‘। " 90 100 110 120 130 140 150 Abundance #4732: N-Acetylpyrrolidone 43
7.80 8.00 8.20 8.40 8.60 5000 m/z 124.95 11.74% 99 127 56 86 30 | --mm 1111111111 111 69 112 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66531: Ethanol, 2,2,2-trichloro- । । । ri । । । । ' Ti 1 1 i 1 1 1 ' i 1 ' ' 31 7.80 8.00 8.20 8.40 8.60 m/z 98.90 8.61% 5000 49 77
... .. 1. 61 TII’ I| 84|.......................113Illi.......... I I | f 1 < I | I I I I | I I I I | I I I I | I I I I "[ > 1 ii | n i i | I । < । | I I ri । । । I I p~r r I | 150 11237 | i i I I [ i i । । j‘ i i i [ i i i i—।—।—r m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 7.80 8.00 8.20 8.40 8.60
9451.D GCMS0507.M Thu May 09 14:43:31 2002 Page 2
NYC-WTC_000045524
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NYC-WTC_000045480
Laboratory report documenting GCMS analysis of sample AE09448 including surrogate recovery data conducted on May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045462
Laboratory report documenting GCMS analysis of sample AE09447 including surrogate recovery data conducted on May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046303
Laboratory report documenting GCMS analysis of sample AE09586 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046284
Laboratory report documenting GCMS analysis of sample AE09585 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045498
Laboratory report documenting GCMS analysis of sample AE09449 including surrogate recovery data conducted on May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045443
Laboratory notes describing re-extraction and re-analysis of sample AE09391 due to initial recovery issues on May 15, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046321
Laboratory report documenting GCMS analysis of sample AE09587 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046266
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE09580 on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043716
Analytical report for sample AE08934 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043667
Summary of GC/MS analytical results for sample AE08838 processed on May 7, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046340
Laboratory report documenting GCMS analysis of sample AE09334 conducted on May 8, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015093
Laboratory report documenting GCMS analysis of sample AE12285 with surrogate recovery data and identification of unknown compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000045396
Department of Environmental Protection GCMS analysis record for the World Trade Center site dated May 3-8 2002.
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NYC-WTC_000045397
Single fragmented page from a Department of Environmental Protection record dated May 3, 2002 with illegible content.
Filed in the same folder
NYC-WTC_000045400
GCMS blank analysis report for sample AE09447 listing compounds below detection limits from May 8, 2002.
Filed in the same folder
NYC-WTC_000045411
GCMS calibration report for sample AE09447 showing recovery percentages for various compounds from May 8, 2002.
Filed in the same folder
NYC-WTC_000045415
GCMS reference standard report for sample AE09447 showing quantified compound levels from May 8, 2002.
Filed in the same folder