GCMS analysis results for sample AE10434, May 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAY1002\10434.D vial: 31 Acq On : 11 May 2002 7:21 pm Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.20 2.55 ug/1 155165 1,4-Dichlorobenzene-d4 12.16

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 74 2 2-Acetylthiazole 127 C5H5NOS 024295-03-2 9 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 5 4 Ethanol, 2,2,2-trichloro-______ 148 C2H3C130 000115-20-8 4 bundance Scan 345 (8.202 min): 10434.D (-) m/z 43.05 100.00% 43

5000

' i 1 ' 1 ■ i ' ' ' 1 i ' ' ' 1 i ' ' ■ ' i ' '

m/z- > 10 20 30 37 ■ ’ i ■ 1 1 1 1 1 1 1 1 1 1 - 40 x 50 61 60 I । ■ I ' 1 ■ 1 i 1 70 821k_ 97Il . , 80 90 100 110 117 ,125I,I, , 117 120 130 7.80 m/z 124.95 8.00 8.20 8.40 12.24% 8.60

Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 7.80 8.00 8.20 8.40 8.60 m/z 46.95 11.45% 15 | ■ ■ । ■ * ■ ■ । 35 ■ i ■ •' ■ ■ । । 49 85 97 117 125 ■ i ■' ■ ' i ■ 11' ।1 1 ' ' । ■ । ' ।' ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4717: 2-Acetylthiazole 43 AAMAA 7.80 8.00 8.20 8.40 8.60 5000 m/z 126.95 9.91% 99 127 58 112 85 33 1—1— 'l ' 1 1 1 I 1 1 1 1 I 1 ' 1 1 I 1 11 1 I ‘ ' 1 1 I TTIBmuum m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4732: N-Acetylpyrrolidone 43 7.80 8.00 8.20 8.40 8.60 m/ Z 97.00 9.15%

5000

99 127 56 86 30 m/z—> ' i' '''11111 11 10 20 30 4 40 69 ITT 1 i ■ ' ' ' i ■ 50 60 70 l.... 111211011———* 90 100 110 120 130 80 7.80 8.00 8.20 8.40 8.60

10434.D GCMS0510.M Thu May 16 10:58:35 2002 Page 2

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