GCMS analysis results for sample AE04128, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\4128.D Vial: 24 Acq On : 23 Mar 2002 6:44 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.30 0.33 ug/1 35784 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 25 2 4,5,6-Try-O-acetyl-2,3-di-O-methyl- 331 C14H21NO8 059061-07-3 9 3 2-Acetylthiazole 127 C5H5NOS 024295-03-2 5 4 N -Acetylpyrrol idone 127C6H9NO2 000932-17-2 5 Abundance Scan 354 (8.297 mln): 4128.D (-) m/ z 43.00 100.00% 43

5000

125 ‘11‘‘+*I‘‘‘‘I**‘SI9T 61 85 99 8.00 8.20 8.40 8.60 1 Tp ’— II ft II m/z 124.85 '1 ‘ 1 1 • 13.05% miz-> 20 40 60 80 100 120 140 160 180 ‘266 220 240 '260' Abundance #12247:2-Propanone, 1,1.1-trichloro- 43

5000 ■ ■ i • ■ • ■ i ■ ' i ■ ■ ‘ ■ i ' ' 8.00 8.20 8.40 8.60 15 m/z 46.85 9.76% 85 97 125 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 ' Abundance 47002: 45 —Th-Oecely-2 3-0.0 metatmennon fe 43 MALMLAL 8.00 8.20 8.40 8.60 5000 m/z 98.85 8.53% 85 99 14127 110 141 159 187 201 261 m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 ' Abundance #4717:2-Acetylthiazole -r-r-p-r-r-r-j-r ' ‘ I 1 1 1 1 1 1 ' 43 8.00 8.20 8.40 8.60 m/z 127.00 8.17% 5000 A 58 99 127 85 112

m/z-> • । • • > • । I 20 40 60 80 100 h • * । ■ ■ -k ■ 111 ■ ■ 1 ■ ■ ■ ■ i ■ ■ ■ ■ । 120 • i ■ •111111' 11'1' 1'1111 140 160 180 200 220 240 260 ■ ' i 1 1 • ■ i ■ 8.00 8.20 ' 1 I ■ ■ ■ ■ i 1 • 8.40 8.60

4128.D GCMS0308.M Wed Mar 27 10:04:16 2002 Page 2

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