GCMS calibration table with surrogate recovery data, Feb 24, 2002

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Calibration table page listing internal standards and response factors for GCMS analysis.

NYC-WTC_000009619–000009628

Folder label: “GCMS X 1/14/02 A 3/4/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB2102\942.D Vial: 64 Acq On : 24 Feb 2002 7:05 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

8.36 0.37 ug/1 23166 1,4-Dichlorobenzene-d4 12.33

Hit# Of 5 Tentative ID MW MolForm CAS# Qual - ----------------- 12-Propanone / 1,1,1-trichloro- 160 C3H3C130 000918-00-3 25 2 Nonane, 4,5-dimethyl- 156 C11H24 017302-23-7 5 3 2-Acetylthiazole 127 C5H5NOS 024295-03-2 5 4 N-Acetylpyrrolidone 127 C6H9NO2 —m/z .95 100.00% 4 000932-17-2 Abundance Scan 361 (8.360 min): 942.D (-) 43

5000 . r । . .vr । , 36 83 97 117 125 8.00 8.20 8.40 8.60 8.80 m/z-> 10 ■ ■ i ■ ■ ■ ■ ।

20 1 ■ i ■ ■' ■ i'

30 40 hyoanoyoanayaanngUmguah 50 60 70 80 90 100 110 120 130 140 150 160 Il.................... ....... i111111'" i1 “ ■ i > * * * । *.. 11. ।* m/z 124.85 10.41 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43

5000 8.00 8.20 8.40 8.60 8.80 15 m/z 96.95 8.50% I 35 85 97 117 I25 ■ • i ■1 “ i “ '11 11111 rl111 TTOIT■ i ■1 ‘ ‘ i ■ •1 ■ i' ‘111 • ■i' • • ■ i • ■ ■11 ■ ■ ■ ■ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #4 162 None ' i din y 43 57

71 8.00 8.20 8.40 8.60 8.80 5000 85 m/z 46.85 8.41%

99 156 113 126 “ I * • ‘ 1 | 1 * ' ‘ I ‘ ‘ ‘ * I 1 ‘ ‘ * I 1 * ' * I' ’ “ I “ * ‘ I ‘ 1 1 ‘ I ’ 1 '"11 ' । i । i i i i | i i ri । i i > i । i i n । i i n । i i m/z-> 10 20 30 40 _50 60 70 80 90 100 110 120 130 140 150 160 Abundance #4717:2-Acetylthiazole 43 8.00 8.20 8.40 8.60 8.80 m/z 126.90 7.71% 5000 99 127 58 85 112 33 I....... I "i apaaBapaag “ i “ ‘11 “ *' i ‘ “ * i > “ i “ “ 1 “11 “ ■ ri * < * * । * *»* । <1 * ^ । < * miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 8.00 8.20 8.40 8.60 8.80

942.D GCMS0208.M Fri Mar 01 09:13:20 2002 Page 2

NYC-WTC_000009625

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Instrument output displaying calibration data and surrogate recovery results for sample AE03283.

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