GCMS calibration table with surrogate recovery data, Feb 24, 2002

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Calibration table page listing internal standards and response factors for GCMS analysis.

NYC-WTC_000009619–000009628

Folder label: “GCMS X 1/14/02 A 3/4/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report > • Data File : C:\HPCHEM\l\DATA\FEB2102\942.D Vial: 64 Acq On : 24 Feb 2002 7:05 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.92 1.33 ug/1 109064 Naphthalene-d8 15.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 Benzeneethaamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 47 3 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H22O3Si2 003789-85-3 38 4 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 35 Abundance Scan 1076 (14.924 mln): 942.D (-) m/z 73.0,0 100.00% 73

5000 267 355

45 . 108 133 1 54 1 77193207223 251 14.60 14.80 15.00 15.20 323339 I ■ i * * —mPmmugueamg—emT i * ■ * ■ i TIWNInu m/z 267.00 39.26% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.60 14.80 15.00 15.20 m/z 355.05 32.33% 191 207 251 323 339 111" 1111 ■' i ■ ■' ■ i'' ■ ■ i ■ ■ • ■ i " ■ ■ i ■ " ' i ■ ‘• i' “ ■ i ■ • •' i " ■' i' TTBUIImn—TTTT ITT rn/z->.... 40 60 80 100 120 .140 160 .180 200 220 240 260 280 300 320 340 360 Abundance i *: 73

14.60 14.80 15.00 15.20 ' ' 5000 m/z 356.05 11.26% 267 44 151 179194209 250 TIT ’1****1’4*)**+41*’+41’1*+14*/*1’***14*’’1’’’1’4*22***I’’’’I’’’’I’’+}’’’’I+E m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72300: Benzoic acid, 2-[(trimethylsilyloxy]-, trimethylsi 73 14.60 14.80' 15.00 15.20 ‘ ' m/z 268.00 10.30% 267 5000

45 135151 175 193 299 233249 .................... . 92 m/z~> 40 60 80 100 120 140 160 180. 200 220 240 260 280 300 320340 360 14.60 14.80 15.00 15.20

942.D GCMS0208.M Fri Mar 01 09:13:25 2002 Page 3

NYC-WTC_000009626

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