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GCMS reference standard results, April 2002

Machine-extracted title · confidence 100%

Reference standard analysis results for volatile organic compounds recorded on April 2, 2002.

NYC-WTC_000058609–000058617

Folder label: “GCMS X 3/6/02 A 3/30/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\3016.D Vial: 15 Acq On : 30 Mar 2002 4:51 am Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 ■ Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.84 0.74 ug/1 128032 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 .2 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H22O3Si2 003789-85-3 37 3 BenzeneetHanamine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37 4 N-(Trifludroacetyl)-N,O,O',0' '-tetr 553 C22H42F3NO4Si4 000000-00-0 35 ' Abundance Scan 1067 (14.843 min): 3016.D (-) m/z 73.00. ’1007b0% 7|3

5000 267

45 108 133 154 177193 223 251 , 323 339 355

I ......M........- 14.60 14.80 15.00 15.20 rW m/z 267.00 44.39% ill?-?___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl ....... 73

5000 267 355 A . 14.60 14.80 15.00 15.20 m/z 355.0 37.94% 323 339 I 191 207 m/z->___ 40_ 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72300: Benzoic ac:d 2-l(trfnett)yisilyl)oxyi-7lrimcthyisi i 73 ' ' I ' -pT-r 14.60 14.80 15.00 15.20 267 5000 m/z 356.05 13.74% 45 92 T-rT-p-ry-ryTT-ri-YTrrrYrT-rTy^ P' " I m/z->__ _40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 ...340 360 Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyijmethyiene] ....... .......... ! 7l3 14.60 14.80 15.00 15.20 m/z 268.0.0 10.81% 5000 267 44 ! 151 179194 209 250 I ' ' ' ' I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20

3016.D GCMS0308.M Tue Apr 02 11:02:35 2002 Page 1

NYC-WTC_000058616

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NYC-WTC_000058616Source: NYC Law Department, mirrored locally

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