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Document / 15 pages

GCMS analysis results for sample AE02647, Mar 15, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02647.

NYC-WTC_000005448–000005462

Folder label: “GCMS X 2/5/02 A 3/7/02

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Scanned page image, NYC-WTC_000005456
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0702\2647.D Vial: 20 Acq On 8 Mar 2002 8:25 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.89 0.43 ug/1 68905 Naphthalene-d8 15.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasilox .e, decamethyl- 370 C10H3005Si5 000541-02-6 58 2 Benzoic acid, 2/ -[ (trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 38 3 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38 4 3,4 -Dihydroxy enzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 35 Abundance Scan 1073 (14.892 min): 2647.D (-) ' m/ z 73.00 100.00% 73

5000 267 355 | i ■ • ■ ■ । । । ■ i > । 45 14.60 14.80 15.00 15.20

m/Z-> 1 ‘I’’ 40 108 mPPm I f T 1

60 251 - 133 154 177 193207 223 323 339.. 4 . | ■ m/ z 267.0 0 39.45% M 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 I Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000 267 , , . .. .... 1. i____ 14.60 14.80 15.00 15.20 ; m/z 355.05 34.16% 191 207 251 323 339 li, miz-s 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 73

14.60 14.80 15.00 15.20 267 I m/z 3 56.0.5 5000 12.65% 45 92 135151 175 193 209 233249 m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyljmethyiene] 73 14.60 14.80 15.00 15.20 । m/z 268.00 10.05% 5000 267

m/z-> M44

40 60 III 151 179194 209 250 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 .. n. . 14.60 14.80 15.00 15.20

2647.D GCMS0208.M Wed Mar 13 14:58:18 2002 Page 2

NYC-WTC_000005456

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NYC-WTC_000005456Source: NYC Law Department, mirrored locally

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