NYC-WTC_000022953
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 8 pages
GCMS calibration data for TCLP method, May 2002
Machine-extracted title · confidence 100%GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
NYC-WTC_000023055–000023062Folder label: “GCMS X 5/8/02 A 5/9/02”
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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\MAY0302\9570.D Vial: 44 Acq On 5 May 2002 10:09 am Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.79 5.04 ug/1 462199 Naphthalene-d8 15.83 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74 2 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 38 3 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 4 Benzoic acid. 4-[(trimethylsilyl)ox 282 C13H2203Si2 002078-13-9 37 Abundance ' Scan 1064 (14.792 min): 9570.D (-) m/z 73.10 100.00% 73
5000 267 355 45 14.40 14.60 14.80 15.00 15.20 — 108 154 193 223 293 323 ‘*14 "1* ri*it 11111111 i 1 ■ । ■ ■ ■ ■ । ■ ' ■ • । 1 1 1 1 i 1 1 m/z 267.05 29.90% mz-> 50 100 150 200 250 300 350400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 27.36% 207 | 323, J............... ■ ■ i * . ... 1 niz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls 73 355 1 '11 1 1 1 1 1 1 I ' 1 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.10 10.04% 45 147 179 223, 267 297 mlz-> 50 100 150 200 250 300 350 400‘450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 14.40 14.60 14.80 15.00 15.20 355 rn/z 74.10 8.59% 5000
45 208 251 281 ! 386 458 548 ■ ■ । ■ 1 1 ■ । ■ III/I’oj i 1 ' ' ■ i 1 ' 1 ' i ' ■ ' ' I '' ' 1 ' I ' 1 r ' i r ' ..... .................. m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20
9570.D GCMS0501.M Tue May 07 15:00:27 2002 Page 2
NYC-WTC_000023061
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