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← Document results/DEP Box 14/GCMS X 1/14/02 A 3/4/02
Document / 10 pages

GCMS analysis report for sample AE01155, March 2002

Machine-extracted title · confidence 95%

Analytical results page for sample AE01155 processed on March 4, 2002, showing surrogate recovery data.

NYC-WTC_000009692–000009701

Folder label: “GCMS X 1/14/02 A 3/4/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB2102\1155.D Vial: 67 Acq On : 24 Feb 2002 10:01 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.92 0.82 ug/1 70175 Naphthalene-d8 15.97

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl - 000541-02-6 64 370 C10H3005Si5 2 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Benzoic acid, 2,5-bis (trimethylsilo 370 C16H30O4Si3 003618-20-0 37 .. .. .. ..... . —. . . N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 4 Benzeneethanamine, .. Abundance Scan 1076 (14.923 mln): 1155.D (-) m/z 73.0,0 100.00% 73

5000 267

. 45 355 ...... m 14.60 14.80 15.00 15.20 “ i ■ “ • i ■ ■ I, 108 133 154 177 193 . , 223 ................. .............. m/z 267.00 36.55% m/z~> 40 60 ‘ 80 100 120 140 160 180 200 220 240 260 280 300. 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 14.60 14.80 15.00 15.20 m/z 355.0 30.86% 191207 251 । 323339 m/z->40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance"..... . 73 , ..... ........... 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 12.25% 44 88 130147 193 267 294 'I ' TTTmMTTI* । > i i! । n ri j i 11 । i rrp i 11 | i i n 11 n i | ri n । ... . । > . । . i i . |. 11 . । .... ।.... f mfe->____ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ... Abundance” #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-. trimethyls 73 14.60 14.80 15.00 15.20 ' ' 355 m/z 268.00 9.80% 5000 45 I 147 179 207 223 , nImwanuumnnunmTPTummmmEuuu 267282297 111111111 if1 11370 ri ।,

m/z~>__ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20

1155.D GCMS0208.M Fri Mar 01 09:08:57 2002 Page 2

NYC-WTC_000009700

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NYC-WTC_000009700Source: NYC Law Department, mirrored locally

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