GCMS analysis report for sample AE01155, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1155.D Vial: 67 Acq On : 24 Feb 2002 10:01 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R..T. EstConc Area Relative to ISTD R.T.

8.19 4.35 ug/1 285381 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual —------------ 1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 1,3-Dio7xolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 343 (8.194 min): 1155.D (-) 73 m/ z 73.00 100.00%

5000 43 7.80 8.00 8.20 8.40 8.60 38.1, J 50 5,5, , , । , 11.' ■ • i 1 ■ 87 l'‘ i ■ • ■ ■ i 103 ■ i ■ m/z 43.05 30.90% m/z-. 10__ 20___ 30 _40___ 50 _ 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000 44 58 7.80 8.00 8.20 8.40 8.60 ......................... ............................... m/z 41.05 11.43%

m/z->_____ 10 15 ' ■ i ■ ■ ■ ■ i * 20 1, 30 1 ।11 ‘ I' i . । . . 40 50 60 i ■ • ■ ■ i

70 ■ 1 ■ ■ ।

80 ■ ■ ■ ■ i

90 ■ ■ ■ ■

100 । • ' ■ •

110 i ■

Abundance ” 73

7.80 8.00 8.20 8.40 8.60 5000 43 m/z 44.95 11.38%

■ • i ■ • ■ ■ i * ■ ■ ' m/z->____ 10 . 20___ 30 Abundance

5000 27 58

i ■ ■ ■ ■ i ■ • ■ ■ i ' 1'1 1 i ' 1 1 1 i 1 1 1 1 i ' 1 1 ' i 1 1 1 1 i 1 1 1 1 i 1 40 50 60 __ 70___ 80. _. 90___ 100__ .110 #62932: Silane, tetramethyl- 73 87

...................... — 7.80 m/z 8.00 71.0.0 L 8.20 8.40 7.23% 8.60

45 15 , J 53 59 1.88....................... ‘ ' i ■ ‘ i • ■ ■ 1 i ■ ■ ■ • i । 1 1 1 I i i । > । । ■ i ■ ■ ■ ■ । ■ • ■ ■ । ■11 ■ i11111 ■1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

1155.D GCMS0208.M Fri Mar 01 09:08:53 2002 Page 1

NYC-WTC_000009699