GCMS analysis report, sample AE04508, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\4508.D Vial: 15 Acq On : 22 Mar 2002 1:06 am Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.14 2.13 ug/1 368430 1,4-Dichlorobenzene-d4 12.27

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

I N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 4 Silane, tetramethyl-________ _ 88 C4H12Si_ __ 000075-76-3 9 Abundance Scan 337 (8.137 min): 4508.D(-) m/ z 73.00 100.00% 73

5000 43

87 103 7.80 8.00 8.20 8.40 , |, | 50 55 . 67, । 1 111111111* 1 I । । 1 ■ I '■■'''.'I । । i • i • ■ ■ • i ■ ■ 1 ■ i ■ ■ ■ ■ i • ■ ‘ ■ i ■ ■ m/z 43.05 29.68% miz-> 10 20 30 40 50 60 70 80 ..-90___ 100 110__ 120 Abundance #292: N-Ethylformamide 30

5000 73 . V TTI Or r Ti-4 ■ । । IITTT r । [ 7.80 8.00 8.20 8.40 44 58 m/z 45.05 10.53% 15 IIIImT ■ " vyle, i ■ 1 ■ ■ i ■ 1 ■ ■ i ■ 1 ■ ' i ■ ' ' ■ i 1 ■ ■ ■ i ■ • ■ ■ i ■ ■ m/z-> 10 20 30 40 !50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane. 2d bremo-5,5 5-i ch j02,2dmet 73 _____ .______ ______ _ ■ ■ i ■ • ‘ ’ i ■ ■ ■ • i • ■ 1 ■ i ' ■ ■ • i 7.80 8.00 8.20 8.40 5000 m/z 41.05 10.38% 45 36 55 67 109115 ■ ■ i ■ ■ ‘ । ■ ■ ■' । ■ ■ ■ • । ■ • ■ ■ । ■ i ■ ■ ■ ■ i ■ ■ ‘ • i' ■ ■ • i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ • ■ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63573: 3-Pentanol, 3-methyl- . ri ' imn di na 1 . r । 73 7.80 8.00 8.20 8.40 m/z 71.00 6.84% 5000 55 27 45 87 ' ‘ l ' ' ' ' l ‘ | 39, I 1 ... ,1 ................ ' I ' ‘ ' 'I' • ■ ■ । ■ • 1 ■ !’*’I* 1 ’ ‘ 1 1 • ‘ » I ’ • ’ 1 I ’ ‘ ‘ I ‘ ‘ ‘ I ' * 4 J k l . » I J I J 1 I I I I I J "8 m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40

4508.D GCMS0308.M Fri Mar 22 09:45:59 2002 Page 1

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