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GCMS analysis report, sample AE04508, April 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry results for sample AE04508 analyzed on April 4, 2002.

NYC-WTC_000012391–000012401

Folder label: “GCMS X 3-1-02 A 3-21-02

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Scanned page image, NYC-WTC_000012399
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2102\4508.D Vial: 15 Acq On : 22 Mar 2002 1:06 am Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Octanol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.24 0.35 ug/1 60779 1,4-Dichlorobenzene-d4 12.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Octanol 130 C8H180 020296-29-1 23 2 3-Hexanol 102 C6H140 000623-37-0 17 3 2-Propanone, 1-eye1opropyl- 98 C6H10O 004160-75-2 9 4 5-Hexen-2-one 98 C6H10O _ 000109-49-9 9 Abundance/ Scan 348 (8.238 min): 4508.D (-) m/z 43.05 100.00%| 43

59 5000 101 1 -r 1 pT4 i I • 11TT IPr 83 88 7.80 8.00 8.20 8.40 8.60 mmmmpmmpl +14 TTHpm m/z 59.05 58.79 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120

_A Abundance #5530: 3-Octanol 59

5000 83 7.80 8.00 8.20 8.40 8.60 31 m/z 100.95 23.09 44 101 mmTTTTTTTTTTT | 112 rn/z~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #63531; 3-Hexenoi 59 i ■ ‘ ■ i ■ -A-— ’ I**}* 7.80 8.00 8.20 8.40 8.60 5000 73 m/ z 58.0 5 15.55 43

qjpaspgygqg , 11.. 11,. ।.... ।.... (..., । > >.. ],. I,,....,.,,, ।. m/z~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 [Abundance #1306:2-Propanone, 1-cyclopropyl- . M.AM 43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 7.785 5000

55 29 mmHm Tmphhn . i i 69 > . I | 1 I l 1 | > > . . | 83 98 . I < | H l>| i > I i | i I l 1| I > > I | , ■ . ■ | i . > . |> > > > | i -rfn 1 , m ri ri n . miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 7.80 8.00 8.20 8.40 8.60

4508.D GCMS0308.M Fri Mar 22 09:46:04 2002 Page 2

NYC-WTC_000012399

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NYC-WTC_000012399Source: NYC Law Department, mirrored locally

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