GCMS analysis results, sample AE05235, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5235.D Vial: 46 Acq On : 31 Mar 2002 1:36 pm Operator: Sample : gc/ms scan 3/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-1-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.96 0.43 ug/1 52415 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanoy, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 Silane, tximethyl- 74 C3H10Si 000993-07-7 37 3 3-Hexanol 102 C6H14O 000623-37-0 37 4 Methane,/ diethoxy- 104 C5H12O2 000462-95-3 33 A£uniteno8...... . .... 7.. ...... ................. S'can 753 (11.961 min): 5235.D (-) m/z’..."59 Jo 5 ipyTm /

5000 45 103 73

4i 86 I 11.60 11.80 12.00 12.20 m/z 45.00 45.70% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 'Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 5l9

5000 45 103 J 4 11.60 11.80 12.00 12.20______ 73 31 m/z 103.05 40.55%' i i ‘rn-rr I ...................130 m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 iAbundance #62564: Silane, tnmelhyl- I 59

11.60 11.80 12.00 12.20 5000 73 m/z 73.00 33.58%

15 31 45 I I im/2-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance ■ #63529: 3-Hexanol rA ... 5|9 11.60 11.80 12.00 12.20 m/z 41.05 5.74% 5000 31 73

I 44 ! 4 .....................102.............. I \a, , 1^ , IM , 10 20 30 40 50 60 70 80 90 100 110 120 130 11.60 11.80 12 00 12 20

5235.D GCMS0308.M Wed Apr 03 14:01:20 2002 Page 3

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