GCMS reference data for sample AE04038, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\4038.D Vial: 19 Acq On : 23 Mar 2002 1:47 pm Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.15 3.76 ug/1 417312 1,4-Dichlorobenzene-d4 12.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 4 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance .. . Scan 338 (8.145 min): 4038.D (-) m/ z 73.00 100.00% 73 5000 43 ■ ' I 1 1 ■ 1 I ■ ■ ■ ■ r' 187 । । > । । । i 87 103 7.80 8.00 8.20 8.40 50 55 ' ' I ’ • 1 ‘ 1 1 ‘ * ry-r-r 38 1 38,441 . । . *——nru ।67,1। i 1 ■ ■ i ‘ • »'» । . । ‘। . m/ z 43.05 26.98% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 i 73

5000 ■ ' i ■ 1 ‘ I’’ > । । । T1 rri i । i 44 58 7.80 8.00 8.20 8.40 m/ z 41.0,5 10.01% 15 ■ ‘ i ■ 1 ■ • i ■ —1 ■ —TT . j f T“. r { । । । । m/z-> 10 20 30 40____ 50____ 60। 70 80 90 100 110 Abundance " slane ■ Gms 0 v 73 __। . > i ___ t J > । —An t » r'l ............... । i । । i 7.80 8.00 8.20 8.40 5000 m/z 45.05 9.75% 45 15 53 59 -*11*n—nk——n———n.nm—B—-Fuor . . * i *| . . . j . . . 88. _____________ । . . . . । . . . . । . m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573:3-Pentanol, 3-methyl- ■ ‘ i ■ ' ■ ■ i 1 1 ' 1 i ' 1‘”l i 1 1 1 1 i 1 73 7.80 8.00 8.20 8.40 m/z " 7.25% 5000 55 45 87 27 ‘ ' i ‘ I ' i ■ ' ' ■ i ■ ' ■ 391 I4 ' ■ ' i ■ ' । ■ • । ■ l • > t • । । । . ' ' I ‘ ‘ ‘ ' I ' ‘ ' I 1ini I 1 1 ' 1 I ' m/z~> 10 20 30 40 50 60 70 80 90 100 110 _ 7.80 8.00 8.20 8.40

4038.D GCMS0308.M Wed Mar 27 10:00:06 2002 Page 1

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