GCMS calibration data for sample AE07484, April 2002

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Data File : C:\HPCHEM\l\DATA\APR1802\7484.D Vial: 17 Acq On : 20 Apr 2002 9:11 am Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.11 0.30 ug/1 36312 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1,3 -Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 4 3-Pentang1, 3-methyl-_______________ 102 C6H140 000077-74-7 9 Abundance Scan 334 (8.111 min): 7484. D (-) m/ z 73.00 100.00% 73

5000 43 1 ■ ■ i ' 1 1 r । r' 1 1 । ■ 1 ■ । 1 1 1 1 । 7.80 8.00 8.20 8.40 ......... 87 103 ’ '.5'.... i 1 ' ' 1 i ,5 ' ' i ' ' ' ' i 1 ’ ' 1 i ' ■ ' ',1,148 1 i ' ' 1 '.i ' 1 m/ z 42.95 27.12% m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide

5000

15 33

44 58 73

1 ' ' 1 1 '

m/z 7.80 _A 41.05 8.00 8.20 ' 1 i 1 1 ■ 1 i 8.40 12.23% I - • 1 t 1 1 1 1 I 1 , i1, | 1 I 11 1 1 I 1 1 1 1 i 1 1 1 1 I 1 1 1 '"I 1 1 1 1 r1 rn/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902:1,3-Dioxolane, 2-methyl- 73 .. MA 1 ■

7.80 i 1 ■ 1 r

8.00 i 1 ■ A 8.20 ' 1 । 1 1 ■ ■ । 8.40 5000 43 m/z 44.95 10.26% 58 27 87 1 I | r i i i । i i i i | i i i i । I 1... T । । । i | • I r i | i i I I 1—I I I j I I I ITT m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- I I I j-1 I I , I f I I I I I I I I ‘ I" I I 7)3 7.80 8.00 8.20 8.40 m/z 71.00 6.32% 5000 45

27 33 39 1 55 ■ ■ । ■ ■ ■ ■ । ■ i > । । । । < । । < । m/z~> 10 20 30 40 50 60 70 80 9o' 100 110 7.80 8.00 8.20 8.40

7484 .D GCMS0419.M Mon Apr 22 12:35:17 2002 Page 1

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