Calibration record for GCMS analysis using standard compounds, generated on April 19, 2002, to ensure instrument accuracy.
NYC-WTC_000044279–000044288Folder label: “GCMS X 4/23/02 A 4/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
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Data File : C:\HPCHEM\1\DATA\APR1802\7484.D Vial: 17 Acq On : 20 Apr 2002 9:11 am Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 14.81 0.26 ug/1 40427 Naphthalene-d8 15.84 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6(91 2 3,4-Dihydro: benzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 52 3 Noradrenali e, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 N- (Triflu -oacetyl)-N,0,0',0'1-tetr 553 C22H42F3NO4Si4 000000-00-0 37 Abundance Scan 1064 (14.813 min): 7484.D (-) m/z 73.00 100.00% 73
267 355 5000
45 14.40 14.60 14.80 15.00 15.20 i /| ।'i i i i '| i193 i 154 — 323 , I" " I ii । i\ i i । i i I । । i i | ■ i'"1 'i'" !‘*111‘111111011111 m/z 267.00 50.52% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 / \ 5000 । 1 1 1 1 । ■ 1 1 ' i 1 ■ ‘ ' । ■ ' ■ ' । 1 1 14.40 14.60 14.80 15.00 15.20 m/ z 355.05 49.78% 1‘I‘ 1 (TTpy ! > | ! I I I | I I > I | 207 < I | .>> <| ..........11 11323 -p-n-v] vr.. । ... TTT—TrTr71"I । , । r 1" r "' i m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73
14.40 14.60 14.80 15.00 15.20 267 m/z 356.05 19.35% 5000 179 356 45 147 "I''"i' L '| | 209 237, T’TTp i""i""I"" I, ‘ 1 ' ' ’ 1111 "| 1 "> | 312 f1" I"1' i" " i"111 p-rf mlz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #57357: Noradrenaline, tetra-TMS (tttI" ' ’ ' I 73 14.40 14.60 14.80 15.00 15.20 m/z 267.90 13.50% 5000 102 355
45 147 I 442 i" " i" " i'"1 r " 'r "1 r "1 r "' ।1 ,,Tr1" r ‘ "r111 r1111 T I I I I ' ' I I ' 40 60 80 100120140160180200220240260280300320340360 380400420440 14.40 14.60 14.80 15.00 15.20
7484.D GCMS0419.M Mon Apr 22 12:35:18 2002 Page 2
NYC-WTC_000044285
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NYC-WTC_000045452
Technical document displaying GCMS calibration data and compound retention times for sample AE09391 processed in early May 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046351
Laboratory report showing GCMS calibration data for sample AE09334 generated on April 25-26, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046294
Laboratory report showing GCMS calibration data for sample AE09585 generated on May 4-6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046332
Laboratory report showing GCMS calibration data for sample AE09587 generated on May 4-6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048479
Instrument scan data for GCMS calibration using deuterated standards on April 4, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009619
Calibration table page listing internal standards and response factors for GCMS analysis.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011494
Instrument output displaying calibration data and surrogate recovery results for sample AE03381.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048737
GCMS laboratory report for sample AE05852 analyzed on April 23, 2002, by analyst DLV.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011429
Instrument output displaying calibration data and surrogate recovery results for sample AE03281.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013117
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023718
Laboratory report of GCMS analysis for sample AE10064 conducted on May 23, 2002, showing surrogate recovery data.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011539
Instrument output displaying calibration data and surrogate recovery results for sample AE03383.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044239
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 23 and April 26, 2002.
Filed in the same folder
NYC-WTC_000044240
Fragmented page from a GCMS record series dated between April 23 and April 26, 2002, likely containing analytical data.
Filed in the same folder
NYC-WTC_000044245
Laboratory report of a GCMS blank analysis (Sample AE07484) conducted on May 2, 2002, checking for background contamination.
Filed in the same folder
NYC-WTC_000044253
Calibration report listing quantified values for various organic compounds including nitrosamines and chlorobenzenes used for instrument verification.
Filed in the same folder
NYC-WTC_000044257
Calibration record for GCMS analysis using standard compounds, generated on April 26, 2002, to ensure instrument accuracy.
Filed in the same folder