GCMS calibration data for sample AE07484, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1802\7484.D Vial: 17 Acq On : 20 Apr 2002 9:11 am Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

25.73 0.21 ug/1 37043 Phenanthrene-dl0 25.59

Hit# of S Tentative ID MW MolForm CAS# Qual 1 Phenanthrene -d10// 188 C14D10 001517-22-2 53 2 Anthracene d10- z 188 ' C14D10 001719-06-8 40 3 4 - Fluoro t'S-methyl-2-phenylpyrimidin 188 C11H9FN2 000000-00-0 38 4 Cyclohexanone, phenylhydrazone 188 C12H16N2 000946-82-7 36 Abundance Scan 2253 (25.728 min): 7484.D (-) m/z 188.10 100.00% 188

5000 .... / ' ‘I ' ' 1 1 p < I I f I I I I I I I I I

66 80 94 160 25.40 25.60 25.80 26.00 42 rl i । . i i . | , I , i | I I , i । 111111111" i1 I ’' 1 r I ।' ■11111 ■ 11 ■''' I' 11 ItT m/z 189.10 15.91% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

5000 J 25.40 25.60 25.80 26.00 m/ z 94.00 12.63% 80 94 160

m/z-> 40 50 60 66 70 80 l I'' ‘11 11 1 11''' 11 90 100 110 120 130 140 150 160 170 180 190 ...iij....,..... I<,,. Abundance #19957: Anthracene-d10- 188 - I ' 1 1 ' I 1t* 1 I 25.40 25.60 25.80 26.00 5000 m/Z 184.00 10.01%

66 80 9|4 160 ] I । I I | ) i I । | i r i i | I I i n I i i | i > i I | I I I I | I I I I | I I I I | I I I I | I I I I | I I '111'1 ’1 r m/z->____ 40 50 60 70 80 90 100 110 120 130 _140 150 160 170 180 190 Abundance #19858: 4-Fluoro-6-methyl-2-phenylpyrimidine 108 .. 1 25.40 25.60 25.80 26.00 m/z 80.05 9.00% 5000 85 103 51 7 n ‘ t । । i pi < > । । । i i । । i ri i । i ■ .84, 114 173 | i । | i I । i j-1 ri i । i । i Itu-vuim [ r । i i । r i i r ।' I I p r | i i li | i i m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

7484.D GCMS0419.M Mon Apr 22 12:35:19 2002 Page 3

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