GCMS calibration data for sample AE07484, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1802\7484.D Vial : 17 Acq On : 20 Apr 2002 9:11 am Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,3-Cyclohexanedione , 4-propyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

33.28 0.39 ug/1 54342 Chrysene-dl2 33.64

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,3-Cyclohexanedione, 4-propyl- 154 C9H14O2 018456-81-0 32 2 Phenol, 3-fluoro- 112 C6H5FO 000372-20-3 27 3 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 25 4 1-Decene, 4-methyl- 154 C11H22 013151-29-6 23 Abundance Scan 3076 (33.283 min): 7484.D (-) m/ z 57.00 100.00% 57 1 2 70 43 5000 83 239 257 ......... 97 129 157 185 | || 33.00 33.20 33.40 33.60 IT ,'i,1.l < ,,, 1' ।,1 7 । >1 m/z 112.10 92.62% m/z—>40 60 80 100 120 140 160 180 200 220 240 260 Abundance #10817:1,3-Cyclohexanedione, 4-propyl- 1 2

5000 55 70 84 k' ' 1 33.00 33.20 33.40 33.60 A TI A

42 m/ Z 70.10 71.16% 97 i 1 । i| । i 1 i । i r| , 125 154 I I r I I I I I 1 I I I I I I I I I I I I [ I I I I I I I I I I I I I I I I 1 i 1 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #2494: Phenol, 3-fluoro- 1 2 . I ' ' 33.00 33.20 33.40 33.60 5000 m/ z 71.00 63.43% 83 64 37 49 | ’ I’/’ * i 1 1 1 i 95 1 ''' i 1 1 ’ I" I -l I I ’V+ i I I I_I l l l ~l _ I' I I I I I I I I I I I I r I I I

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester A— 57 33.00 33.20 33.40 33.60 70 m/ z 43.05 57.61% 5000 83 112

42 — 98 ....... .. ......... ..... ii | 199 217 i 1 1 ’ ■ i ■ 1 i 1 1 1 I 1 1 '■ I 1 11 1 I 1 1 1 ' TOdi I I I I I I I I l' I I I I I I I I I ' 1 i 1 1 1 ' i ' r 1 1 i ' 1 ‘ ■ i ■ ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 33.00 33.20 33.40 33.60

7484.D GCMS0419.M Mon Apr 22 12:35:20 2002 Page 4

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