GCMS analysis results for sample AE05852, April 23, 2002

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GCMS laboratory report for sample AE05852 analyzed on April 23, 2002, by analyst DLV.

NYC-WTC_000048737–000048757

Folder label: “GCMS X 4/11/02 A 4/15/02”

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Data File C:\HPCHEM\1\DATA\APRO4 02\5852.D Vial: 26 Acq On 4 Apr 2002 10:44 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Propanedioic acid, hexyl-, die Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 33.32 8.97 ug/1 263283 Chrysene-dl2 33.68 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 38 2 1,2-Cyclopentanedione, 3-methyl- 112 C6H802 000765-70-8 16 3 Octane,/ 2-chioro- 148 C8H17C1 000628-61-5 16 4 Isooctane, (ethenyloxy)- 156 C10H20O 037769-62-3 12 Abundance Scan 3080 (33.323 min): 5852.D (-) m/z 57.00 100.00%) 57 112 70 43 5000 83 239 256 --------- 97 33,00 33.20 33.40 33.60 4 , 'ilk ill , t/, / 129 ■ 143 157 171■ 185 199 213 227 ' I ■ ■ • 281 IE — T '■ i i ‘ ■ i • ‘ i • i ' 1 ‘ i ‘ i • ■ ' ■ i ■ ■ m/z 112.10 84.23% n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 2«) 280 Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 70

5000 . y *1 11, 1 i 83 112 33.00 33.20 33.40 33.60 m/z 70.10 72.69% 42

mlz-> 20 H40 i ■ ■ • • t 60 80 98 I J......................... 199 217 .... ................. 100 120 140 160 180 200 220 240 260 280 Abundance #2500: 1,2-Cyclopentanedione, 3-methyl- 112 ‘ ‘ i • 1 ■ ‘ i • 1 ' ‘ i ‘'r ■ ■ i ' r‘ ■ i 33.00 33.20 33.40 33.60 5000 55 69 m/z 71.00 70.43 83 27 42 1 i ‘ ‘ I -- ' 144 ‘ T" 97 1 1 ‘ ‘ ‘ ‘ 1 1 ‘ ‘ ‘ I ‘ ‘ ‘ ‘ I ‘ ‘ ‘ I 1 1 ‘ ‘ I ' ‘ ' r| ‘ ‘ ' | । । । ' | ‘ ‘ mte-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #66554: Octane, 2-chloro- 70 33.00 33.20 33.40 33.60 55 m/z 43.05 63.72% 83 5000 42 27 112 97 i____ 11444144 * 11 * * ' i ■ 1 • ■ i 1 ' ‘i ‘ ‘1 i11 ■ ■ i • ' ‘ ‘ i ■ ■ ■ ■ I ■' ■ ■ i‘' i ■ ■ ‘ ■ i ‘ ‘ 1 i ■ ITTPrit mfz~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 33.00 33.20 33.40 33.60

5852.D GCMS0408.M Tue Apr 16 08:18:33 2002 Page 2

NYC-WTC_000048756

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NYC-WTC_000048756Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE05846, April 23, 2002 · Box DEP Box 27

NYC-WTC_000048717

GCMS laboratory report for sample AE05846 analyzed on April 23, 2002, by analyst DLV.

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