GCMS method 508 scan data, March 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\4849.D Vial: 6 Acq On : 29 Mar 2002 7:55 pm Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Propanedioic acid, hexyl-, die Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

33.33 5.77 ug/1 607030 Chrysene-dl2 33.70

Hit# of 5 Tentative' ID MW MolForm CAS# ■Qual

1 Propanedioic acidXhexyl-, diethyl 244 C13H24O4 005398-10-7 38 2 Cyclohexane, (1 dimethylpropyl)- 154 C11H22 031797-64-5 25 3 Octane, 1., 1'-ojf-ybis- 242 C16H34O 000629-82-3 22 4 Tridecane, 7-methyl- 198 C14H30 026730-14-3 22 Abundance Scan 3081 (33.328 min)?4849.D (-y m/ z~112 710 ■■‘■'"10 0 70 0 % 70 1 2 43

5000 83 I I

'Abundance I 20 40 60 JLIa 80__ 1.00__ 120 143 ''57 171 185 199 213 227 ' I ' ' ' ' I ' ' ' ' I 140 160 180 #32687: Propanedioic acid, hexyl-, diethyl ester ' I ' ' 200 239 256

‘ I ' ' ' ' I 220 240 .......... . 260 33.00 33.20 33.40 33.60 m/z 57.0,0 99.89%

70

5000 83 112 33.00 33.20 33.40 33.60 m/z 70.10 83.17% ■ ' 98 199 217 ti I I

'm/z-> 20 40 60 80 100 120 ' 140 160 180 200 ^20 240 260 Abundance #11064: Cyclohexane, (l.l-diir.ethyloropyi). i 76 I ' ' I ' 33.00 33.20 33.40 33.60 5000 m/z 71.1 0 .75.58% 27 83 125 •i 97 139 154 m/z-> 20^40^60.80 100 120 140 160 180 200 220 240 260 Abundance #71251: Octane, l.l'-oxybis- 57 71 33,00 33.20 33,40 33.60 m/z 71.50% 5000- 84 i 42 112

. :m/Z“> 20 ....... I I ' ' ' ' I ' 40 u 60 I 80 100 120 143 140 160 180 200 210 224 220 240 260 33.00 33.20 33.40 33.60

4849.D GCMS0308.M Tue Apr 02 11:03:40 2002 -Page 3

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