GCMS analysis results for sample AE05852, April 23, 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1202\5852.D Vial: 7 Acq On : 15 Apr 2002 1:57 pm Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Propanedioic acid, hexyl-, die Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 33.30 4.37 ug/1 608307 Chrysene-dl2 33.67 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Propanedioic acid, hexyl-, diethyl 244 C13H2404 005398-10-7 38 2 Hexane, 2,3-dimethyl- 114 C8H18 000584-94-1 35 3 Hexane, 3,3,/-trimethyl- 128 C9H20 016747-31-2 35 4 1-Butanol, -methyl-, carbonate (2: 202 C11H2203_ _____ 002050-95-5 35 Abundance Scan 3078 (33,300 min): 5852.D (-) Tm/z 57.00 100.00% 57 112 70 43

5000 83 239 256 97 33.00 33.20 33.40 33.60 miz-> o+— 4 li k A11** -***1 nL-1-1 20 40 60 80 100 120 140 160 180 200 220 240 260 129 143 157 171 185 199 213 227 96.87% Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 70

5000 11 Pin i' 83 112 33.00 33.20 33.40 33.60 m/ Z 70.00 78.15% 42 98 it . | 199 217 1 1 ' ' ' I I ■ 1 ’ ■ i 10/1/n/n/1/n///nn——n/nuuuwtrrani miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #3097: Hexane, 2,3-dimethyl- 43 1 • i ■ ■ —— 70 33.00 33.20 33.40 33.60 5000 m/z 71.00 73.64% 27 55 — 85 114 11411 I1 ' ■ i ■ 1 • ■ i ■ ■ • ■ i ' ' ‘ 1 i ■ 1 ■ ■ I 1 1 1 ' I ' 1 1 1 I 1 1 ' ' I 1 ' 1 ' I 1 1 1 1 I ' ' iz—> 20 40) 60 80 100 120 140 160 180 200 220 240 260 Abundance #65108: Hexane, 3,3,4-trimethyl- TIT T 43 57 71 33.00 33.20 33.40 33.60 m/z 43.05 67.43%

5000

27 99 — ' ‘ I11' ' 1 12,7 1 .......... I 113............................................................................ J ‘ i * ■ ■ ■ i • ■ ■ ■ i ' • ■ ' i ■ • ‘ ‘ I ' ' 1 1 1 1 ‘ 1 ' I ' ' ■ 1 1 1 1 1 1 1 1 1 1 1 I ' 1 Tamr • ■ i ‘ ■ 1 ■ I 1 1 1 1 I ' 1 n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 33.00 33.20 33.40 33.60

5852.D GCMS0412.M Tue Apr 16 15:40:38 2002 Page 5

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