GCMS chromatogram data for sample AE04594, April 2002

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Library Search Compound Report

Data File : C:\HPCHEiyi\l\DATA\MAR2602\4594.D Vial: 10 Acq On : 26 Mar 2002 6:37 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Propanedioic acid, hexyl-, die Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

33.32 0.54 ug/1 63650 Chrysene-dl2 33.70

Hit# of .5 Tentative / ID MW MolForm CAS# Qual

1 Propanedioic ap-id, hexyl-, diethyl 244 C13H24O4 005398-10-7 38 2 3,3-Dimethyl-2^hexanol 130 C8H18O 022025-20-3 35 3 Trifluoroacetyl-3,7-dimethyloctanol 254 C12H21F3O2 000000-00-0 32 4 2-Undecene, -^methyl - , (Z) - 168 C12H24 074630-45-8 22 Abundance SmiH 36m (33:321 .... m/ z 7 70 1 2 43

5000 83 ------ 1 I I I I I I A / I ■T^i-i'^i-r-i-i-A4-i-[- 97 239 256 __ 33.00 33.20 33.40 33.60 129................................... , , , IL . . A m/z 112.10 97.63% 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #32687: Propaneciioic acid, hexyl-, diethyl ester

70

5000 83 112 33.00 33.20 33.40 33.60 m/z 70.10 89.83% 42 ^1 199 217 m/z-> 20 40 60 80 100 120 140 160 180 200220 240 260280 Abundance #5560; 3,3-Dirne;hyl-2-he.xanoi 43 70

33.00 33.20 33.40 33.60 5000 55 m/ Z 43.05 77.05%

27 ■ 1 101

m/z->.. 20.. 40.. 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #34655: Trifluoroacetyi-3,7-dimethyloctanol 43 33.00 33.20 33.40 33.60 55 70 m/z 71.10 74.36% 5000 83 27 i I ..LjLIl 125 -n- 140 169....................... m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 33.00 33.20 33.40 33.60

4594.D GCMS0308.M Thu Mar 28 16:30:02 2002 Page 2

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