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GCMS analysis results for sample AE08951, May 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE08951 conducted on April 29, 2002, including detection of unknown compounds.

NYC-WTC_000043619–000043631

Folder label: “GCMS X 3/26/02 No Analyses

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0602\8951.D Vial: 8 Acq On 6 May 2002 11:10 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L **************************************************** * ** * * * * * * * * * * * * ** Peak Number 5 Propanedioic acid, hexyl-, die Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

36.13 0.89 ug/1 45561 Perylene-dl2 37.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Propanedioic/acid, hexyl-, diethyl 244 C13H2404 005398-10-7 27 2 1-Decene, 2,4-dimethyl- 168 C12H24 055170-80-4 17 3 Octane, 1,1/-oxybis- 242 C16H340 000629-82-3 14 4 2-Undecene, 4,5-dimethyl - , [R@,S@-( 182 C13H26 055170-93-9 12 Abundance ( Scan 3392 (36.126 min): 8951 .D (-) m/z 185.15 100.00% 185 57 70 5000 41 — 112 83 98 1 1 i 1 ■ ' i ' 1 1 1 i । 143 209 35.80 36.00 36.20 36.40 - I I T 1 .1 281 m/z 57.10 70.85% m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 __ Abundance #32687: Propanedioic acid, hexyl-, diethyl ester 57 70

5000 ■ ■ i ■ ■ 83 112 35.80 36.00 36.20 36.40 m/ Z 70.05 56.14% 42 98 | 199 217 fl ,i i । i । i i । n । । । i i i i । । > । > । ki । । । iiii । > । । । । i । । । । । । I 1 1 1 ' I i 1 11 ■ i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #14795:1-Decene, 2,4-dimethyl- 43 57 A........ 1 ' i 1 1 ■ ' i

83 35.80 36.00 36.20 36.40 5000 m/ Z 71.10 49.04% 70 112 97 1........ 168...................... i ■ ■ 1 1 i' 1 ।11 ■ ■ । 1 '' i 1 1 ' ' i ' ■ ' 1 i 1 1 ' ' i ' 1 ' 1 i 1 ' 1 1 1 1 1 ' 1 1 1 ' 1 1 i 1 1 1 ■ i 1 ■ r ■ i r 1 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #71250: Octane, 1,1’-oxybis- 57 35.80 36.00 36.20 36.40 43 71 m/z 41.15 41.75%

m/z-> 5000 27

1’’’’ I1 ' 20 40 + 60 84

ML 97 143 80 112 1 1 1 1 11 1 I ' 1 1 ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ > ■ ■ । 100 120 140 160 180 200 220 240 260 280 224 ■ r ■ । ■ ■ ■ ■ । • I ■ ■ ■ ■ । ■ aAA 35.80 36.00 36.20 36.40

8951.D GCMS0501.M Wed May 08 11:51:43 2002 Page 5

NYC-WTC_000043630

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NYC-WTC_000043630Source: NYC Law Department, mirrored locally

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