GCMS analysis results for sample AE08951, May 2002

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Data File C:\HPCHEM\l\DATA\MAY0602\8951.D Vial: 8 Acq On 6 May 2002 11:10 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Hexadecanoic acid Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

28.08 0.48 ug/1 45300 Phenanthrene-dl0 25.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecanoic acid 256 C16H3202 000057-10-3 38 2 .alpha.-D-Galactopyranoside, methyl 194 C7H14O6 003396-99-4 17 3 1,6-Anhydro-.beta.-D-glucopyranose 162 C6H10O5 000498-07-7 12 4 Dodecanoi acid 200 C12H2402 000143-07-7 12 Abundance / Scan 2514 (28.080 min): 8951 .D (-) m/ z 43.10 100.00% 43 60

5000 102 73 256 85 120 239 r i | i i > I | CvUI [ i iii [ I r

27.80 28.00 28.20 28.40

m/z-> I 1—I-1 T L 401 4 ldlaIl 601 80 100I 115

120 ।

140 157 171 185

160 180 200 213

220 240 260 m/z 60.00 66.72% Abundance #71607: Hexadecanoic acid 43 60 73

5000 256 11 1 i 1 1 1 1 i ' 1 129 27.80 28.00 28.20 28.40 85 97 213 m/ Z 41.10 52.82% 157 171 I 227 i 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #21079: .alpha.-D-Galactopyranoside, methyl 60 ——————————— 27.80 28.00 28.20 28.40 74 5000 m/z 57.05 50.08%

L. 31 87 103 116 131 145 163 I I - m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #12774:1,6-Anhydro-.beta.-D-glucopyranose (levoglucosan) 60 27.80 28.00 28.20 28.40 m/z 102.15 48.18%

5000 73

31 42 I II | ,, l|, 85 98I ■ 1 1 i ■ r - 1 1 1 m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 27.80 28.00 28.20 28.40

8951.D GCMS0501.M Wed May 08 11:51:42 2002 Page 4

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