GCMS analysis results, sample AE05234, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5234.D Vial: 45 Acq On : 31 Mar 2002 12:37 pm Operator: Sample : gc/ms scan 3/9 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Hexadecanoic acid Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

27.37 0.37 ug/1 61891 Phenanthrene-dl0 25.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecanoic acid 256 C16H32O2 000057-10-3(^4 2 Tetradecanoic acid 228 C14H28O2 000544-63-8 72 3 Tridecanoic acid 214 C13H26O2 000638-53-9 72 4 Pentadecanoic acid 242 C15H30O2_ 001002-84-2 59 'Abundance 60 73 Scan 2431 (27.366 min); 5234.D (-) m/ z ■73.00". “looToo^ 43 I I 5000 129 ^■1 |||„ ,1 I ?5 97 115 256 143 213 27.00 2L20 27.40 27.60 I I II, m/z 60.05 95.75% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #71609; Hexadecanoic acid i 40 60 73

5000 4^ 27.00 27,20 27.40 27.60 129 97 213 256 m/z 43.05 79.43% i 157 171 185 i J II I I I 199 i 227- m/z--> :20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #f084i; Tetradocanoic acid t 60 73 i 27.00 27.20 27.40 27.60 5000 m/z 41.05 73.20% 129 27 85 185 228 •I : I 97 :il 'I 143 171 I l\ f\i\ K J m/z--> 20 40 60 80 100 120 140 160'180 200 220 240 260 Abundance #70343; Tridecanoic acid I 73 27.00 27,20 27.40 27.60 m/z 57.00 65.04% 5000 129 27 85 214 I ^'7, ,,,l , , ,n A 'm/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 27.00 27.20 27.40 27.60

5234.D GCMS0308.M Wed Apr 03 13:59:29 2002 Page 5

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