GCMS analysis results, sample AE05234, April 2002

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Laboratory report documenting GCMS analysis of sample AE05234 for unknown compounds on April 9, 2002.

NYC-WTC_000059156–000059171

Folder label: “GCMS X 3/9/02 A 3/30/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5234.D Vial: 45 Acg On : 31 Mar 2002 12:37 pm Operator: Sample : gc/ms scan 3/9 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator)' Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Cholestanol Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

39.89 4.18 ug/1 266149 Perylene-dl2 37.93

Hit# of 5 Tentative ID MW .MolForm CAS# Qual

1 Cholestanol 388 C27H48O 000080-97- 2 7-Oxabicyclo[4.1.0]heptane, 1-methy 168 C10H16O2 000096-08-■2 12 3 Cyclohexane, 1,5-diethenyl-2,3-dime 164 C12H20 068779-14-6 11 4 1,E-11,Z-13-Heptadecatriene 234 C17H30 080625-35-0 11 Abundance Scan 3795 (39.888 min):'5234.D’(-) ”m/z "215'. 15 "10 0.00% 5(5 2 5 81 107 149 233 5000 133 355^^3

/n/z-> Abundance 3 Il I YYyTTTYpnn-rp-T--rrp-r 331 3i9

40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 MUUfcw #74154: Cholestanol AiXitr 39.60 . 39.80 40.00 40.20 m/z 55.00 93.67%

2t5 233 107 .165 5000 123 147 388 39.60 39.80 40.00 40.20 m/z 81.05 82.47% 355 262 I I 1

40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 'Abundance #14555: 7-Oxafcicyclo[4.1.dJheptane, l-niethyi-4-(2-nicttiytoxi I 43

39,60 39,80 40.00 40.20 5000 m/ z 43.00 81.69% 67 93 109 inz ......................................................................................................................................................................................................................................... ............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................. ■

jn/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #13592: Cyclohexane, l\5-dietheny|/2.3-<^rnethyP.’(taTph^ .. ................... ' ' ' 1 ' ' ' < I • I 107 39.60 39.80 40.00 40.20 79 m/z 95.00 75.84%

5000 135

I 164 '40 60 TO' 160 '120 140 160 '180 260 220 240 260 280 3oo' 320 '340 '360' 380 ' 39.60 39.80 40.00 40.20

5234.D G.CMS0308.M Wed Apr 03 13:59:33 2002 Page 6

NYC-WTC_000059168

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GCMS analysis results, sample AE05235, April 2002 · Box DEP Box 57

NYC-WTC_000059172

Laboratory report documenting GCMS analysis of sample AE05235 for unknown compounds on April 9, 2002.

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