GCMS analysis results, sample AE05234, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5234.D Vial: 45 Acq On : 31 Mar 2002 12:37 pm Operator: Sample : gc/ms scan 3/9 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 Coprostan-3-one Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

40.52 3.60 ug/1 228812 Perylene-dl2 37.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Coprostan-3-one 386 C27H46O 000000-00-0 58 2 Pregnane-/, 20-dione, (S.beta.)- 316 C21H32O2 000128-23-4 30 3 Cholesterol 386 C27H46O 000057-88-5 15 4 1-Naphth41enecarboxylic acid, decah 3 16 C21H32O2 015798-13-7 12 Abundance Scan 3864 (40.521 min): 5234.D (-) m/z 55.00 100.00% 81 231 161 386 5000 105122 316

»n/z~> Abundance 1' .lUWwaX 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #52763: Coprostan-3-one 353 '. ..I..).l..l„. 40.20 40.40 40.60 40.80 m/ z 43.05 98.72%

43

5000 231 .... 386 40.20 40.40 40.60 40.80 67 95 i 1, 123 161 m/z 231.10 76.62% 316 I IIh 368 'm/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #45159: Precnane-3.2G-dicne. (S.beta )- 43 / jA 40.20 40.40 40.60 40.80 5000 m/z 81.05 74.75% 84- 246 1 107 “8 316 : I 135 159176 213 272 m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 'Abundance #74135: Cholesterol 43 40.20 40.40 40.60 40.80 m/ z 95.00 73.72% 107 149 386 5000 213 275 301 255 353 I I » I I 3 AA A 40 60 80 100 120 140 160 180'200 220 240 260 280 300 320 340 360 380 40.20 4g,40 40.60 40.80 |

5234.D GCMS0308.M Wed Apr 03 13:59:38 2002 Page 7

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