GCMS calibration table for method GCMS0412, April 2002

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Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.

NYC-WTC_000047701–000047714

Folder label: “GCMS X 4/4/02 A 4/12/02”

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Data File : C:\HPCHEM\1\DATA\APR1102\8016.D Vial: 22 Acq On : 12 Apr 2002 11:02 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 Cholestanol Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 39.84 2.38 ug/1 183983 Perylene-dl2 37.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cholestanol 388 C27H480 000080-97-7 (93 2 Epicholestanol 388 C27H480 000516-95-0 30 3 Epicoprostanol 388 C27H480 000000-00-0 12 4 5.alpha.-Cholest-22-ene, (Z) - 370 C27H46 015076-93-4 11 Abundance Scan 3790 (39.839 min): 8016.D (-) m/ z 43.05 100.00% 43 81 2 5 .I107 149 233

| 5000 124 373 AA A AAA A 2 282 331 3f5 ' ' ' I ' 1 ' ' I ' ' ' ' T ' ' ' 'I 175193 n/z-> TTpT II IL r'' "i"v 11' ■ ■ ''1 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 T’I| ,I I.... I |....... J..... I ’T | | [ r 1 i 1 | 1 1 Fi | 1 1 I I | I rl 114 I I 7 j I I I I | I m/ z 39.60 39.80 40.00 40.20 81.05 96.19% Abundance #74154: Cholestanol 2)5233

107 165 A / 5000 388 39.60 39.80 40.00 40.20 , 147 124 m/z 215.15 94.59% 262 355 ............................ | " i " " r '" i " ■' rT" I' ■ " i1' " r 1" i'1 n I" 1 " ' r 1" i " 1 T’i n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #52986: Epicholestanol 215 233 388 A 39.60 39.80 40.00 40.20 5000 m/z95.00 85.60% 165 107 355 262 ll I I 331 m/z-> r '111" " r " ■ i r " ' i " " i " " r " ' i' " r i' " i 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 TI‘T3 1" " r "1111" 1 4 i ■r 1 ■ i

Abundance #52981: Epicoprostanol 43 215 39.60 39.80 40.00 40.20 m/z 55.00 82.63%

5000 370 95 388 165 233 I—188 316 “ITE"PCP—I"TUDmEuu1I —u UUTTI rI | । । TI| I I I ( | I I IT ' > 1 1 ■ 1 r | 1 1 > ■ । A—AA ■ /z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 39.60 39.80 40.00 40.20

8016.D GCMS0412.M Tue Apr 16 12:08:09 2002 Page 6

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