GCMS calibration data for method 508, April 23 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \ HPCHEM \ 1 \ DATA\APR2 202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 Cholestanol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

39.80 4.04 ug/1 440896 Perylene-dl2 37.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cholestanol 388 C27H480 000080-97-7 74 2 Epicholestanol 388 C27H480 000516-95-0 38 3 Epicoprostanol 388 C27H480 000000-00-0 35 4 Indan, 6-tert-butyl-4-ethyl-l,1-dim 23 0 Cl7H2 6 003247-65-2 9 Abundance Scan 3786 (39.800 min): 8757.D (-) m/z 215.15 100.00% 2 5 55 81 107 149 233 5000 124 373 331 355 i TT -pi rrrj-i-r

4 443 A 18) +©1 I । । 257 288 39.40 39.60 39.80 40.00 40.20 — ‘‘1 I I I I I I I t I I I I I I I ■ I m/z 81.05 82.71% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #74154: Cholestanol 2 5233

107 165 5000 TAM 1 1 1 1 1 1 ' 1 1 1,1 1 11 388 39.40 39.60 39.80 40.00 40.20 147 m/ Z 55.00 80.99% 24 262 355 11 r ■ ■1111' ■ i111 ■ rT'1 r " ■ r 1 " i1" ■ 11 ‘11111 ■ i * H ................ | i1" ' r ‘1 r i1" 111 TTT T’I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #52986: Epicholestanol 215 203 388 | I I I I | I i i । | “T “I r r । I i i i । i i

39.40 39.60 39.80 40.00 40.20 5000 m/ Z 95.00 80.76% 165 107 355 262 I I 331 111111111111 ■111" 11 r ' " i1 ■ " i" 1' i ' i11" Pv TT 11 " 11 -rp-r- I 1 1 1 1 I I " '' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #52981: Epicoprostanol AM ...... 1a 1111yp) AAA 43 215 39.40 39.60 39.80 40.00 40.20 m/z 43.00 76.68% / 5000 370 95 388 165 233 ............. J.............. | | । 188 | । l........... 316.... 1... _ i " ‘ ■ i1" 1 r 1 ■' r 1" r " 1111111 ‘ " 1 r ■ ‘1111 , Ti i iii । । “I । । । । । । । । । i । । । । । । I | । । । । । ri"i * । rir i । r ‘ T m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 39.40 39.60 39.80 40.00 40.20

8757.D GCMS0412.M Tue Apr 23 08:23:09 2002 Page 16

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