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GCMS calibration data for method 508, April 23 2002

Machine-extracted title · confidence 100%

Calibration data for GCMS analysis of volatile organic compounds recorded on April 23, 2002.

NYC-WTC_000044313–000044337

Folder label: “GCMS X 4/23/02 A 4/26/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2 202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 15 2-Hexyl-1-octanol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 32.28 0.37 ug/1 51314 Chrysene-dl2 33.64 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexyl -1 octanol 214 C14H30O 000000-00-0 43 2 2-Hexyl-1 -decanol 242 C16H340 000000-00-0 38 3 Ethano, 2 - (tetradecyloxy)- 258 C16H34O2 002136-70-1 38 4 1,2-Octadecanediol 286 C18H38O2 020294-76-2 35 Abundance Scan 2967 (32.282 min): 8757.D (-) m/z 57.00 100.00% 57

5000 41 71 83 07 97 111,25 139 154

1 280 32.00 32.20 32.40 32.60 4,. ‘i l, /L, ___ , J 1,154167 182 m/ z 41.05 1 114 ' 1 r1 1 • [ I I I 1 I I ' II I II 1 1 I I I 1 I | I I t I | I I F I | I ! I I | I I I I | I 36.96% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #26413: 2-Hexyl-1-octanol 57

MWW/ MV VyMAy 71 5000 32.00 32.20 32.40 32.60 85 97 111 m/z 71.00 34.86% ■ I 11111 1 1 h 1 II 125 i T i । II i i । i r I I । 168 i i i i । I i 196 । । । i t i । । i ■ i i । i i i i | I I I I | I I ‘ 1 I ' 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #32422: 2-Hexyl-1-decanol 57

32.00 32.20 32.40 32.60 71 m/z 5000 43.00 34.64% 85 97 111

1 1 1 1 ' —— ,125 139 .............196 I I I | I I I I | I I I I [ । I r I | I i i i i “ i' i 224.................. i [l i i II i I-1 | 1l i 1 4 | I T wAMNV __ m/z-> 40 60 80 100I 120 140 160 180 200 220 240 260 280 Abundance #71663: Ethanol, 2-(tetradecyloxy)- 57 32.00 32.20 32.40 32.60 m/ z 97.05 30.91% 71 83 5000- 97 111 125 10 TTII1 TIT 'll | | 224 258 1 1 i 1 —————————————— m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 32.00 32.20 32.40 32.60

8757.D GCMS0412.M Tue Apr 23 08:23:08 2002 Page 15

NYC-WTC_000044333

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NYC-WTC_000044333Source: NYC Law Department, mirrored locally

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