Calibration data for GCMS analysis of volatile organic compounds recorded on April 23, 2002.
NYC-WTC_000044313–000044337Folder label: “GCMS X 4/23/02 A 4/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR2202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Hexadecanoic acid Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
27.33 1.60 ug/1 300094 Phenanthrene-dl0 25.59
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Hexadecanoic acid 256 C16H3202 000057-10-3 2 Tetradecanoic acid 228 C14H28O2 000544-63-8 68 3 Pentadecanoic acid 242 C15H30O2 001002-84-2 68 4 Dodecanoic acid 200 C12H24O2 000143-07-7 64 Abundance Scan 2428 (27.333 min): 8757.D (-) m/z 73.00 100.00% 43 60 73
5000 129 85 97 256 t । । । 1. i । T I i i । r-1 i-1 । । । । t । 157 174 185 213 ...... |l , nj _ -4 1 1 1 ’ 1 r1 1 1 11 1 Il 7 115 143 I I I I 199 I. 227 ■ • i ■ ■ I 111 I I I I I I 1 I I I I I I I I I 11 I I I I t "IB 27.00 27.20 27.40 27.60 m/z 59.95 85.09%
L m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #71609: Hexadecanoic acid 43 60 73
.................. 1*1‘ ‘I’ / 5000 129 27.00 27.20 27.40 27.60 85 97 256 m/z 43.00 81.44%
m/z-> 20 i 1 1 1 1 i ' 40 ' I ' ■ 1 ' । 1 1' 1 ‘ I । I । 1 1 । । ' 60 80 100 120 157 171 15,199 312,227 140 160 180 200 220 240 260 Abundance #70841: Tetradecanoic acid 60 73
27.00 27.20 27.40 27.60 5000 m/ z 41.05 69.65% 129 27 85 185 228 , 97 143 171 | I, J., IiI m/z-> 20 40 60 80 100 120 140 160। 180 200 220 240 260 Abundance #71238: Pentadecanoic acid 60 73 27.00 27.20 27.40 27.60 m/z 57.00 64.38%
5000 129 85 242 97 143 19E 199 | 157 171 | TT 11 J ID ' , _ 1 i ■ 1 1 ' I ' ' ' 1 T 1' ' ' I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 27.00 27.20 27.40 27.60
8757.D GCMS0412.M Tue Apr 23 08:23:07 2002 Page 14
NYC-WTC_000044332
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NYC-WTC_000043238
Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046249
Calibration table data for GCMS analysis of volatile organic compounds dated May 3-6, 2002.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043458
Gas chromatography-mass spectrometry analysis report for sample AE07106 including surrogate compound recovery data.
1 shared topics · Same agency, volume and box · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045526
GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.
1 shared topics · Same agency, volume and box · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048583
Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038642
Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated February 22, 2002.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013943
TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.
1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047701
Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.
1 shared topics · similarity 0.987
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000044239
Single-page administrative log from DEP Box 25 covering GCMS X analyses dated between April 23 and April 26, 2002.
Filed in the same folder
NYC-WTC_000044240
Fragmented page from a GCMS record series dated between April 23 and April 26, 2002, likely containing analytical data.
Filed in the same folder
NYC-WTC_000044245
Laboratory report of a GCMS blank analysis (Sample AE07484) conducted on May 2, 2002, checking for background contamination.
Filed in the same folder
NYC-WTC_000044253
Calibration report listing quantified values for various organic compounds including nitrosamines and chlorobenzenes used for instrument verification.
Filed in the same folder
NYC-WTC_000044257
Calibration record for GCMS analysis using standard compounds, generated on April 26, 2002, to ensure instrument accuracy.
Filed in the same folder