GCMS analysis results for sample AE05898, March 29 2002

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Library Search Compound Report

Data File ; C:\HPCHEM\l\DATA\MAR2102\5898.D Vial: 26 Acq On ; 22 Mar 2002 1:56 pm Operator: Sample : gc/ms scan 3/13 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Hexadecanoic acid Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

28.16 7.87 ug/1 2881160 Phenanthrene-dl0 25.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecanoicz acid 256 C16H32O2 000057-10-3 35 2 Isopropyl yalmitate 298 C19H38O2 000142-91-6 25 3 Hexadecanc^-lc acid, 2,3-dihydroxypro 330 C19H38O4 000542-44-9 22 4 Nonadecanpic acid 298 C19H38O2 000646-30-0 15 Abundance Scan 2518 (28.160 mjn)r5898?Dl^^^ m/ Z 4 3 7'0 5..... Too .00% 4)3 102 60 5000 256 73 129 239 ■ I I > I > I > I <-| pT-i > . I I I

27^0 28.00 28.20 28.40 298 m/z 102.05 69.41% £n/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #35186: Hexadecanoic acid 60 73

5000 ..........I \.......... . , 27.80 28.00 28.20 28.40 129 m/z 60.05 62.05% 157171 185 213 256 tTl/Z-> __ _ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #^248£ iicpiopyl Paln’itate 102

27.80 28.00 28.20 28.40 5000 60 m/z 54.19% .73. 129 . 87 157 I 'r-r-r-p- 257 ■m/z-> . ......... 40_ 60 80.... 100.. 120 140 160 180 200 220 240 260 „280 _J00 Abundance #46899: Hexadecanoic acid. 2,3-dihydroxypropyi esier ■R" 4|3 27.80 28.00 28.20 28.40 m/z 256.25 47.37% 5000 98 60 239

, '?27O ,,111...I,..! I, .I.I.,. I ' ' ' H ' ' ' ' 312 ■R m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 27.80 28.00 28.20 28.40

5898.D GCMS0308.M Mon Mar 25 14:28:34 2002 Page 2

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