GCMS analysis results for sample AE05899, March 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR2102\5899.D Vial: 27 Acq On : 22 Mar 2002 2:55 pm Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Hexadecanoic acid Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T,

28.15 0.67 ug/1 301808 Phenanthrene-dl0 25.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadec loic acid 256 C16H32O2 000057-10-3 38 2 Isopro 1 Palmitate 298 C19H38O2 000142-91-6 27 3 Nonanoic acid 158 C9H18O2 000112-05-0 18 4 OctanZ ic acid, ethyl ester 172 C10H20O2 _ _ 000106-32-1 17 Abundance ' ................... — Saiifi-^ir (287149 min): 5899h (-)" m/ z 4 3 7q5 - - Q Q “q q 413

60 102 5000 73 256 I 83 ............ 239 I UU#. OuJ 129 : 'm/z->40 60 80 ,

100 115

120 I 143 157 171 185 199 213 140 160 180 200 220 240 260 27.80 28.00 28,20 28.40 m/z 102.05 63.22% Abundance #71607: Hexadecanoic acid 4!3 60 7S I- 5000 255 129 _.2ZJ0__28,P0_J8,20_J8,40_^ . p 97 213 m/z 60.05 62.61% II (ju 157 171 I I I 227 40 60 80 100 120 140 160 180 200 220 240 260 i Abundance ■ #42488: Isoprepyi Pa'rnitate ! 102 i 27.80 28.00 28.20 28.40 5000 60 m/z 41.05 56.77% 73 129 85 I 157 257 'ni/z->____ 40___ 60__ 80__ 100__J 20__ 140__ 160__ 180 _ 200 _220 _ 240 260 Abundance #67434: Nonanoic acid............. ... ...... . 73 27.80 28.00 28.20 28.40 m/z 57.0,0 48.08%

I 5000

87 ^p29 l| I ,,l I i.... 158...................... 80 100 120 140 160 180 200 220 240 ' 260 -r—T- mZz-> 40 60 27.80 28,00 28.20 28.40

5899.D GCMS0308.M Mon Mar 25 14:29:33 2002 Page 2

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