GCMS analysis results for sample AE01331, March 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\1331.D Vial: 20 Acq On : 22 Mar 2002 6:01 am Operator: Sample : re-extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Hexadecanoic acid Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

28.15 0.25 ug/1 76184 Phenanthrene-dl0 25.67

Hit# of 5 Teiy;ative ID MW MolForm CAS# Qual

1 Hexadecanoic ^cid 256 C16H32O2 000057-10-3 38 2 Isopropyl P^mitate 298 C19H38O2 000142-91-6 14 3 Octanoic Ac^d 144 C8H16O2 000124-07-2 10 4 Octanoic a/cid, silver (1-t-) salt 251 C8H16AgO2 024927-67-1 10 Abundance ' Scan 2517 (28.155 min): 1331.D (-) m/z.... 437o^. iboT^ 43 102 60 5000- 256 73 , ^ , , , , I , , / .............

Ji , ,1 Jl.il I .T .T. I,., 27.80 28.00 28.20 28.40 _____ i .. ' ' ‘ ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' i ' ' ' ' I ' ' ' ' ( ' ' m/z 102.05 62.84% 'm/z->. 20 . 40.. 60 80.. 100 120.. 140 160 180 200 220 240 260 Abundance #71608: Hexadecanoic acid ¥ 57 73 256 »- I / I-,-, 5000 129 27.80 28.00 28.20 28.40 85 97 m/ z 59-9.5 56.81% i I ' ' ' ' I ' 1,1. j... f J 2^,... m/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260

a Abundance #42488; IsoDropvl Palmitate 102

2L80 28.00 28.20 28.40 5000 60 m/ z 41.05 51.46% 73 129 85 I 257, m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 'Abundance #66326: Octanoic Acid 6b 27,80 28,00 28.20 28.40 ! m/z 256.25 41.47% 73 5000 27 45 85 101

m/z-> 20 Il 160,1 '“I ‘ 40 'I ' 80 III 100 120 129, 144........... ..... 140 160 180 200 220 240 260 27.80 28.00 28.20 28.40

1331.D GCMS0308.M Mon Mar 25 14:23:22 2002 Page 2

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