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GCMS analysis results for sample AE01331, March 29 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of environmental sample AE01331 conducted on March 29, 2002.

NYC-WTC_000059708–000059717

Folder label: “GCMS X 3/13/02 A 3/27/02

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Scanned page image, NYC-WTC_000059715
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\1331.D Vial: 20 Acq On : 22 Mar 2002 6:01 am Operator: Sample : re-extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.80 0.21 ug/1 65975 Phenanthrene-dl0 25.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-d/p6'Y 188 C14D10 001517-22-2 83 2 Anthracene-dl/-'/ 188 C14D10 001719-06-8 53 3 Pentacyclo[8/4.0.0(3,7) .0(4,14) .0(6 188 C14H20 000000-00-0 36 4 - (4-Tolyl) -3;-methyl-pyrazol-5-one_ 188 C11H12N2O 035496-19-6 28 Abundance / Scan 2260 (25.795 min): 1331.0 (-) m/z.. 188710..... iooT^O^ 1 ;8

5000-

80 94 5^1 ■ 6,6 ,1 11 132 146 I?® | 25.40, 25.60 25.80 26.00 26.20 m/z 8 .05 14.75% m/z-> 30 40 . 50.... 60.... 70 .. 80.... 9p...JOO . 11 p J20 J30 14p 150 160 170 180 190 Abundance #19958: Phenanthrene-diO 188

5000- r' ' 25.40 25.60 25.80 26.00 26.20

80 94 160 m/z 189.05 14.22% 66 I'''' I'''' I'''' I 'm/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957. Antnracene-d iu- 188 1 25.40 25.60 25.80 26.00 26.20 5000 m/z 9-;: . 00 13.40%

80 94 160 66 ! • I m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19959: Pentacyclo[8.4.6.0(3,7).0(4.14).0(6,11 )]tetradecane 1“^ 1f!8 25,40 25.60 25.80 26.00 26.20 m/z 184.10 11.32% 5000 79 117

‘m/z-> ..... .........t, 131 145 159 ........ I...... I|..... U, 173 I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25:i2- 25.60 25.80 26.00 26.20

1331.D GCMS0308.M Mon Mar 25 14:23:17 2002 Page 1

NYC-WTC_000059715

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NYC-WTC_000059715Source: NYC Law Department, mirrored locally

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