GCMS blank analysis results, April 23, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR2202\LBA.D Vial: 16 Acq On : 22 Apr 2002 11:50 pm Operator: Sample : gc/ms scan 4/12 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 25.73 0.23 ug/1 43410 Phenanthrene-dl0 25.59 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenant hrene-d10 2 Anthrac e-d10- 188 C14D10 188 C14D10 001517-22-2 001719-06-8 64 Q 3 -(4-ToL 1)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 50 4 Naphthalene, 2,6-dimethoxy - 188 C12H1202 005486-55-5 42 Abundance Scan 2253 (25.730 min): LBAD (-) m/z 188.10 100.00 188

5000

40 - 80 94 146 160 25.40 25.60 25.80 26.00T1 — 11 ■' “ i ■ ■ " i “ ■ ■ i " 1' i" '11'' .... llanas m/ z 80.05 15.56%| m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 118

5000 ----- 25.40 25.60 25.80 26.00‛TT m/z 189.05 14.36 80 94 160 .................... 66...... — miz-> 30 40 50 60 70 80 90H100 110 120 130 140 150 160 170 180 190 I' ‘‘ I " ‘ ’ I i “ “ i

Abundance #19957: Anthracene-d10- 188 ' ‘ I ‘ T' ' ‘i r1 1 1 I 25.40 25.60 25.80 26.00 5000 m/z 184.10 12.92

80 94 160 66 । H “ i11" i • • “ i " " i" 1111" ' 11 11-1 miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19863: -(4-Tolyl)-3-methykpyrazol-5-one 144,141 11414L 188 25.40 25.60 25.80 26.00 91 m/ Z 94.10 9.25% 105 5000 119

m/z—> 30 .07 I 146 • ‘d । » j» H i । u j 70 80 90 100 110 120 130 140 150 160 170 180 190 40 50 60 n i i : f q i“1 • i ■ “ ■ i ■■ i ■ ■ “ i “ — j l 25.40 25.60 2580 26.00

LBA.D GCMS0412.M Tue Apr 23 14:25:37 2002 Page 3

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