GCMS calibration table for TCLP method, March 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR0102\3265.D Vial: 40 Acq On : 3 Mar 2002 2:39 am Operator: Sample : gc/ms scan 2/4 fb Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.37 ug/1 101967 Phenanthrene-dl0 25.73

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d 2 Phenanthrenes-diO 277% 188 C14D10 188 C14D10 001719-06-8 80 001517-22-2 80 3 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 53 4 -(4-Tolyiy-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 47 Abundance ( ’ Scan 2266 (25.849 min): 3265.D (-) m/z 18 .10 100.00% 188

5000

94 42 52 66 80 146 156 । | 25.60 25.80 26.00 26.20 ahngaaakapute mhmmpphmtmmmmm m/z 93.90 14.69% m/z-> 40 50 60.. 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 25.60 25.80 26.00 26.20 80 94 m/z 189.10 12.99% 66 160 —mmmmmpt mOPmmmmmmp Trr m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 1 055 Phepanthrene-d0 188 25.60 25.80 26.00 26.20 5000 m/z 184.10 11.41% 80 94 160 66 11'1" 11 i “ 11" ‘1‘‘1/111111/1/1713//2////17//7//1/9:*""13r m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19908: Naphthalene, 2,6-dimethoxy- 188 25.60 25.80 26.00 26.20 173 m/z 7 .95 11.16% 145 5000 102 114 130 76 94 157 nmpp » » j J it i Ttt » I I : I i » | i I ,i__ • i * • n 111 “ (‘1 “ 1111 Im mmmmr 1 ] r l miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

3265.D GCMS0208.M Mon Mar 25 12:16:38 2002 Page 2

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