GCMS analysis results for sample AE03914, Mar 18 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\3914.D Vial: 76 Acq On : 24 Feb 2002 8:48 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L

Peak Number 4 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

25.88 . 0.24 ug/1 22680 Phenanthrene-dl0 25.73

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 91 2 Phenanthrene -d10 188 C14D10 001517-22-2 91 3 Naphthalene,/1,7-dimethoxy- 188 C12H1202 005309-18-2 45 4 3H-Pyrazol-;/3-one, 2,4-dihydro-4,4-d 188 C11H12N2O 017694-06-3 40 Abundance Scan 2269 (25.876 min): 3914.D (-) m/z 188.10 100.00% i 188

5000- -...............— 80 94 160 25.60 25.80 26.00 26.20 i m/z-> 40 44 50 60 70 11 80 4 । • ■ ■ ■ । ■ > ■ ■ । ■ ■ • • । 90 100 110 120 130 140 150 160 170 180 190 —L L ITT m/z 189.10 15.68% Abundance #19957: Anthracene-d10- 188 I i

V 5000 n 25.60 25.80 26.00 26.2 ‘ 80 94 m/z 79.95 14.55% 66 160 ! ■ ' I '' ' ' I ' ' '' I ' ' ' I ' . 1111 > I > I' > I i ■ ■ ■ ■ i mz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 — — 25.60 25.80 26.00 26.20 5000- m/z 160.00 12.69%

II 80 94 160 66 >I 1 ' I ’''' I ■''' I''' ITPPr i ■ ■ ■ ■ i' ■'' i i ■ ■'' i' ■' ■ i i* ■ • 'I 'm/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19913: Naphthalene, 1,7-dimethoxy- ---------------------- 173 188 25.60 25.80 26.00 26.20 m/z 184.10 12.49% 5000- 102 115 145 51 63 75 94 130 TIUPBIa—IITTTTTTTTTe 11 — I 158 I " " i1 - I I t TI miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20 .

3914.D GCMS0208.M Wed Mar 13 11:36:12 2002 Page 4

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