GCMS sample analysis report AE08436, Apr 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1202\8436.D Vial: 25 Acq On : 16 Apr 2002 7:35 am Operator: Sample : gc/ms scan 4/10 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Anthracene-dlO- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 25.75 0.23 ug/1 45152 Phenanthrene-dl0 25.61 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dr0 - 188 C14D10 001719-06-8 87 2 Naphthalene/ 1,7-dimethoxy- 188 C12H1202 005309-18-2 40 3 Phenanthrene-dlO 188 C14D10 001517-22-2 40 4 3-Quinolii/ecarbonitrile, 1,2,3,4-te 188 C10H8N2O2 022384-05-0 38 Abundance Scan 2255 (25.749 min): 8436.D (-) m/z 188.10 100.00% 188

5000

80 94 m 25.40 25.60 25.80 26.00 40 49 " " 111 ‘ ''i'111 r 1111''1' TT 1.1 160 .1...... m/z 80.05 14.39% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

.... —........... 5000 1IlklIIIIIIII I I I I I I I I I I

25.40 25.60 25.80 26.00 m/ z 93.95 14.29% 80 94 160 66 m/z-> mmmmmmT mmm 1 ■ i11" i r 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 188 —

25.40 25.60 25.80 26.00 5000 m/z 189.10 14.13% 102 115 145

51 63 75 94 130 158 “WWTTTTnT mPPT Tilf.. '' ir''11 ■ ■'11' ■ ■ ‘ i ■ | TIr m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 25.40 25.60 25.80 26.00 m/z 184.05 10.51%

5000

80 94 160

miz-> 30 40 50 60 66 70 ll i ■ ■ ■ ■ । ■ ■ ■ ■ । ■ - ■ ■ । - ■ ■ ■ । — 1’ 80 90 100 110 120 130 140 150 160 170 180 190 ■ 111 ■1 ■ 1 i 1 ■ 25.40 25.60 25.80 26.00 11

8436.D GCMS0412.M Wed Apr 17 09:48:33 2002 Page 4

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